# US 6,296,170 B1 · Method of producing metal composites which can be processed at high temperatures

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- Number: US 6,296,170 B1
- Document ID: US6296170B1
- Status: Granted
- Kind: B1
- Application number: 09/425,208
- Filed: 1999-10-22
- Granted: 2001-10-02
- Earliest claimed: 1999-10-22
- Assignees: Sigmabond Technologies Corporation
- Inventors: Roy Hardwick
- Web page: https://patentgrep.com/patent/US6296170B1

## CPC

- B23K 35/005: {at least one of the workpieces being of a refractory metal}
- B23K 20/227: with ferrous layer
- B23K 35/004: {at least one of the workpieces being of a metal of the iron group}
- B32B 15/013: {one layer being formed of an iron alloy or steel, another layer being formed of a metal other than iron or aluminium}
- B23K 35/32: with the principal constituent melting at more than 1550°C
- B23K 2103/24: Ferrous alloys and titanium or alloys thereof
- B23K: SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B32B: LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM

## Abstract

A method whereby a composite clad metal ingot can be produced for onward processing at higher temperatures which are sufficient to allow the properties of the substrate material to be adequately controlled to meet specified requirements. These higher temperatures are required to avoid the undue levels of work hardening which occurs at the lower temperatures previously employed because of the need to avoid the formation of deleterious intermetallics at the bonded clad substrate interface. Such intermetallics are formed at temperatures above approximately 900° C. and should they be present, will weaken or destroy the bond.

## Claims

### Claim 1

A method of producing a composite material, including a layer of metal cladder material and a metal substrate material wherein an interlayer material is interposed between said metal cladder material and said metal substrate material, which comprises bonding said metal interlayer material to said metal cladder material and said metal substrate material, and thereafter hot forming said composite material, said metal interlayer material being such that upon heating said composite material and hot forming at a temperature above 900° C., the bonds between said metal cladder material and said metal interlayer material and between said metal substrate material and said interlayer material are not adversely affected, the interlayer material preventing the formation of intermetallics and depletion of the bond between the substrate material and the cladder material, said metal substrate comprising carbon or stainless steel; the metal cladder material comprising titanium, alloy thereof, zirconium or alloy thereof; and the metal interlayer material comprising niobium, alloy thereof, tantalum or alloy thereof.

### Claim 2 (depends on 1)

A method as in claim 1 in which the metal interlayer material has a melting point higher than the metal cladder material and the metal substrate material.

### Claim 3 (depends on 1)

A method as in claim 1 in which the metal interlayer material is explosively bonded to the layer of metal cladder material and to the metal substrate material.

### Claim 4 (depends on 1)

A method as in claim 1 in which the corrosion resistant metal cladder material is titanium or an alloy of titanium.

### Claim 5 (depends on 1)

A method in claim 1 in which the corrosion resistant metal cladder material is zirconium or an alloy of zirconium.

### Claim 6 (depends on 1)

A method as in claim 1 in which the metal interlayer material is niobium, or an alloy of niobium.

### Claim 7 (depends on 1)

A method as in claim 1 in which the metal interlayer material is tantalum or an alloy of tantalum.

### Claim 8 (depends on 1)

A method as in claim 1 wherein the composite material comprises layers of said metal substrate, metal cladder and metal interlayer materials in substantially flat plate or sheet form to provide a composite flat ingot and said ingot is hot rolled into final sheet or plate form while avoiding the formation of intermetallics between the metal cladder and metal substrate.

### Claim 9 (depends on 1)

A method as in claim 1 wherein the composite material comprises layers of metal substrate, metal cladder and metal interlayer materials of substantially cylindrical form to provide a composite cylindrical billet and the hot forming comprises hot extruding said composite.