# US 6,293,528 B1 · Fractionation apparatus with low surface area grid above tray deck > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 6,293,528 B1 - Document ID: US6293528B1 - Status: Granted - Kind: B1 - Application number: 09/277,072 - Filed: 1999-03-26 - Granted: 2001-09-25 - Earliest claimed: 1998-04-23 - Assignees: Uop LLC - Inventors: Daniel R. Monkelbaan; Michael R. Resetarits; Robert J. Miller - Web page: https://patentgrep.com/patent/US6293528B1 ## CPC - B01D 3/225: {Dual-flow sieve trays} - B01D 3/008: {Liquid distribution} - B01D 3/16: Fractionating columns in which vapour bubbles through liquid (packing elements B01J19/30, B01J19/32) - B01D 3/20: Bubble caps; Risers for vapour; Discharge pipes for liquid - B01D 3/22: with horizontal sieve plates or grids; Construction of sieve plates or grids - B01J 2219/30: Details relating to random packing elements - B01J 2219/32: Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer - B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28) - B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS ## Abstract The flooding capacity of a fractionation tray (2) is increased by the addition of at least one layer of low surface area grids (3) above the inlet to the downcomers (6,12) located on the tray (2). The grids (3) extend upward for a distance equal to one to four times the depth of the downcomers. The grids may rest upon the top edge of the downcomers or on the tray decking between the top portions of the downcomer sidewalls. ## Claims ### Claim 1 A vapor-liquid contacting apparatus comprising: (a) a vertical enclosed column (1) having a circular cross section, an upper first end (20) and a lower second end (21); (b) a plurality of evenly spaced-apart fractionation trays including a pair of vertically spaced apart fractionation trays (2), comprising a lower first and an upper second tray, with the trays being substantially planar and extending horizontally across substantially all of the cross-sectional area of the column (1), and with the trays (2) having perforations (15) evenly distributed across decking sections (5) of the tray (2), which decking sections are devoid of downcomers (12,6); and, (c) a layer comprising low surface area structured grid packing (3) supported by and resting upon an uppermost part of the first tray (2) the first tray (2) of said pair of fractionation trays, with the layer of structured grid packing (3) extending upward toward the second tray for a distance equal to from about one-tenth to about three-quarters of the vertical distance between the first and second trays with the low surface area structured grid packing comprising bent blades (8) having inclined surfaces. ### Claim 2 A fractional distillation apparatus comprising: (a) a vertical enclosed column (1) having an upper first end (20) and a lower second end (21); (b) a pair of vertically spaced apart multiple downcomer fractionation trays (2) comprising a lower first tray and an upper second tray, with the trays (2) extending across substantially all of the cross-sectional area of the column (1), and with the trays (2) having separate vapor passage decking sections (5) and parallel liquid collection downcomers (6, 12) distributed across the trays (2), with the liquid collection downcomers (6, 12) extending away from the tray (2) toward the second end of the column, and with perforations (28) for liquid passage being located in the liquid collection downcomers; and, (c) a layer of low surface area structured grid packing (3) resting upon the first tray of said pair of fractionation trays, the grid packing (3) comprising individual blades (8) having a vertical central portion and inclined upper and lower portions which are inclined on opposite sides of the vertical central portion of the blade, and with the layer of grid packing (3) extending toward the second tray for a distance equal to from about one-tenth to about three-fourths of the vertical distance between the first and second trays (2). ### Claim 3 (depends on 2) The apparatus of claim 2 wherein the layer of low surface structured grid packing (3) extends upward from the first tray for a distance less than one-third of the vertical distance between the first and second trays. ### Claim 4 (depends on 2) The apparatus of claim 2 further characterized in that the layer of low surface area structured grid packing (3) rests upon an upper edge of a downcomer (12) side wall (32), which sidewall holds the layer of low surface area structured grid packing above the upper surface of the vapor passage decking sections (5) of the lower first tray to provide void volumes located between the vapor passage decking sections (5) and the bottom surface of the layer of low surface area structured grid packing (3). ### Claim 5 (depends on 2) The apparatus of claim 2 further characterized in that a bed of packing material (4) is located between the bottom of the upper second tray and the upper surface of the structured grid packing (3) with a cylindrical void volume (v) being located between the bottom of the bed of packing material (4) and the layer of low surface area grid packing (3) is comprised of parallel bent blades, which blades have inclined surfaces and are connected by perpendicular stringers. ### Claim 6 (depends on 5) The apparatus of claim 5 wherein the cylindrical void volume (v) has a height equal to at least {fraction (1/10)}th of the tray spacing between the pair of trays. ### Claim 7 (depends on 2) The apparatus of claim 2 wherein the downcomers have sidewalls having an upper portion which extend upward away from decking sections, and the low surface area grid packing rests upon the decking sections between the upper portion of the sidewalls. ### Claim 8 A fractional distillation apparatus comprising: (a) a vertical enclosed column (1) having a circular cross section and an upper first end (20) and a lower second end (21); (b) a pair of vertically spaced apart discoid fractionation trays (2) extending across substantially all of the cross-sectional area of the column (1), with the trays having separate substantially flat perforated decking sections (5) and liquid collection downcomers (6, 12), which downcomers extend away from the tray (2) towards the lower second end of the column (1), and with additional perforations (17,28) for liquid passage being located in the liquid collection downcomers (6,12); (c) a layer of low surface area structured grid packing (3), resting upon a lower first tray (2) of said pair of fractionation trays; the grid packing (3) comprising a plurality of parallel blades (8) having at least two spaced apart bends yielding inclined surfaces, with the blades being connected by perpendicular stringers and, (d) a layer of high surface area packing (4) located above the layer of low surface area structured grid packing (3). ### Claim 9 (depends on 8) The apparatus of claim 8 wherein a second layer of low surface area structured grid packing (3) is located below the higher tray of the pair of fractionation trays (2), with a cylindrical void volume being located between the lower surface of the second tray (2) and the top surface of the second layer of low surface area structured grid packing (3). ### Claim 10 (depends on 8) The apparatus of claim 8 further characterized in that the liquid collection downcomers (6, 12) comprise triangular cross-section downcomers (6). ### Claim 11 (depends on 8) The apparatus of claim 8 further characterized in that the layer of low surface area structured grid packing (3) rests upon an upper edge of a downcomer (12), which holds the layer of low surface area structured packing (3) above the decking sections (5) to provide a plurality of void volumes located between the decking section and the bottom surface of the layer of low surface area structured grid packing. ### Claim 12 (depends on 8) The apparatus of claim 8 further characterized in that the layer of low surface area structured grid packing (3) rests upon a portion of a downcomer (6) which extends above the flat perforated decking sections (5). ### Claim 13 A vapor-liquid contacting apparatus comprising: (a) a vertical enclosed column (1) having a circular cross section, an upper first end (20) and a lower second end (21); (b) a plurality of evenly spaced-apart fractionation trays including a pair of vertically spaced apart fractionation trays (2) comprising a lower first and an upper second tray, with the trays being substantially planar and extending horizontally across substantially all of the cross-sectional area of the column (1), and with the trays (2) having perforations (15) evenly distributed across decking sections (5) of the tray (2), which decking sections are devoid of downcomers (12,6); and, (c) a layer comprising low surface area structured grid packing (3) supported by an upper portion of a downcomer (12) of the first tray (2) of said pair of fractionation trays, with the layer of structured grid packing (3) extending upward toward the second tray for a distance equal to from about one-tenth to about three-quarters of the vertical distance between the first and second trays with the low surface area structured grid packing comprising bent blades (8) having inclined surfaces. ### Claim 14 A vapor-liquid contacting apparatus comprising: (a) a vertical endosed column (1) having a circular cross section, an upper first end (20) and a lower second end (21); (b) a plurality of evenly spaced-apart fractionation trays including a pair of vertically spaced apart fractionation trays (2) comprising a lower first and an upper second tray, with the trays being substantially planar and extending horizontally across substantially all of the cross-sectional area of the column (1), and with the trays (2) having perforations (15) evenly distributed across decking sections (5) of the tray (2), which decking sections are devoid of downcomers (12,6); and, (c) a layer comprising low surface area structured grid packing (3) comprised of separate bundles having blades (8) aligned in different directions, with the low surface area grid packing being supported by the first tray (2) of said pair of fractionation trays, with the layer of structured grid packing (3) extending upward toward the second tray for a distance equal to from about one-tenth to about three-quarters of the vertical distance between the first and second trays with the low surface area grid packing comprising bent blades (8) having inclined surfaces.