Preparation of bis(3-aminopropyldimethylsilyl)benzene compounds
AssigneeShin-Etsu Chemical Co., Ltd.
InventorsTohru Kubota, Mikio Endo, Yasufumi Kubota
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Abstract
1,2-, 1,3- or 1,4-bis(3-aminopropyldimethylsilyl)benzene is prepared by effecting hydrosilylation reaction between N,N-bis(trimethylsilyl)allylamine and 1,2-, 1,3- or 1,4-bis(dimethylsilyl)benzene in the presence of a platinum catalyst, followed by detrimethylsilylation reaction. The process is simple and inexpensive to synthesize the end compound in high yields without forming isomers.
Claims1
A process for preparing a bis(3-aminopropyl-dimethylsilyl)benzene compound, comprising the steps of effecting hydrosilylation reaction between N,N-bis(trimethylsilyl)allylamine and a bis(dimethylsilyl)-benzene compound of the following general formula (I):
- in the presence of a platinum catalyst, and effecting detrimethylsilylation reaction to form a bis(3-amino-propyldimethylsilyl)benzene compound of the following general formula (II):
- .
Dependencies are inferred from the claim text.