Method of refining benzoic acid
AssigneeNippon Steel Chemical Co., Ltd.
InventorsHiroyuki Kuwahara, Yuji Arifuku, Kazuyoshi Horibe, Nobumasa Noma, Masakazu Takeuchi, Haruki Kawano
Life of this patent
Estimating the term…
Loading patent…
AssigneeNippon Steel Chemical Co., Ltd.
InventorsHiroyuki Kuwahara, Yuji Arifuku, Kazuyoshi Horibe, Nobumasa Noma, Masakazu Takeuchi, Haruki Kawano
Estimating the term…
This invention relates to a process for purifying benzoic acid continuously to a purity of 99.9% or more by introducing crystals of crude benzoic acid with a bulk density of 0.2 g/cm3 or more and an average particle diameter of 0.3 mm or more into a continuous crystallization apparatus equipped with a stirrer and a heating device from the upper portion of the apparatus, effecting counter-current contact of the falling crystals of crude benzoic acid with the melt generated by heating with the heating device, withdrawing the purified benzoic acid as melt from the lower portion of the apparatus, and withdrawing the mother liquor from the upper portion of the apparatus. The process makes it possible to prepare high-purity benzoic acid continuously in a relatively simple apparatus at high efficiency.
A process for purifying benzoic acid comprising:
A process for purifying benzoic acid comprising:
Dependencies are inferred from the claim text.