Method of preparing phosphorus
AssigneeAstaris LLC
InventorRichard R. Severns
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Abstract
A method of producing phosphorus in which a mixture of phosphoric acid and carbon reductant is exposed to microwaves at a power level sufficient to heat the mixture to a temperature at which phosphorous is produced. This method can be carried out at lower temperatures than conventional phosphorous production and does not give rise to the solid waste normally formed in conventional phosphorous production. The phosphorus thus formed can be converted back to phosphoric acid, thus effecting purification of the phosphoric acid.
Claims22
A method of preparing elemental phosphorus, the method comprising:
- (a) heating a mixture of phosphoric acid and a particulate carbon reductant with microwave radiation in a non-oxidizing atmosphere;
- (b) evolving a phosphorous vapor from the mixture;
- and
- (c) condensing the phosphorous vapor to form condensed elemental phosphorus.
A method of preparing purified phosphoric acid, the method comprising:
- (a) heating a mixture of impure phosphoric acid and a particulate carbon reductant with microwave radiation in a non-oxidizing atmosphere;
- (b) evolving a phosphorous vapor from the mixture;
- (c) condensing the phosphorous vapor to form condensed elemental phosphorus;
- (d) recovering the elemental phosphorous;
- and
- (e) converting the elemental phosphorous to the phosphoric acid.
Dependencies are inferred from the claim text.