Process for cleaning bisphenol crystallizer
AssigneeGeneral Electric Company
InventorsRudy Peemans, Jan Huibert Weijland, Mourice Van Sintemaartensdijk
Life of this patent
Estimating the term…
Loading patent…
AssigneeGeneral Electric Company
InventorsRudy Peemans, Jan Huibert Weijland, Mourice Van Sintemaartensdijk
Estimating the term…
An alternative and improved method for cleaning cooling and/or crystallization surfaces of a crystallizer fouled with a crystallized bisphenol as a result of processing a slurry derived from the production of bisphenol is provided. The method includes the steps of: (a) draining from 20 to 80%, and preferably about 50% of the slurry from the crystallizer; (b) replacing the drained slurry with a solvent comprising phenol, thereby forming a diluted slurry; (c) increasing the temperature in the crystallizer to a temperature at which the crystallized bisphenol is dissolved in the diluted slurry, and then rapidly cooling the diluted slurry to a temperature of 45 to 55° C.; and (d) adding a seed slurry containing solid bisphenol at a concentration of 5 to 30%. The seed slurry has a temperature of 45 to 55° C. and is added until conditions are established at which bisphenol crystals added to the crystallizer do not redissolve.
A method for cleaning a cooling or crystallization surface surface of a crystallizer fouled with a crystallized bisphenol, said crystallizer containing a slurry derived from the production of bisphenol, comprising the steps of:
In a method for producing a bisphenol comprising the steps of reacting a first reactant stream containing phenol and a second reactant stream containing a ketone or aldehyde to produce a product mixture containing the bisphenol;
Dependencies are inferred from the claim text.