Device for crystallization by isentropic expansion and its use
AssigneeInstitut Francais du Petrole
InventorsAri Minkkinen, Paul Mikitenko
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AssigneeInstitut Francais du Petrole
InventorsAri Minkkinen, Paul Mikitenko
Estimating the term…
Device and process for crystallizing a component, e.g. paraxylene, from a mixture that comprises a chamber (1) that has in its upper part means (46) for supplying the mixture, collecting means (20), and in its lower part, crystals of the component in suspension in a mother liquor, connected to means (C) for separation and purification of the crystals that are obtained, means (9) for supplying a cold gaseous fluid and means (22) for drawing off the so-called hot gaseous fluid that results from the direct heat exchange, whereby said device also comprises means for shaping a descending flow of the mixture onto tubes such that the cold gaseous fluid that circulates upward exchanges cold directly with the mixture, whereby means (22) for drawing off the hot gaseous fluid are connected to at least one fluid recompression means (24b), whose output is connected to at least one heat exchanger (27), whereby the heat exchanger is connected to a turbo-expander (30), which is connected to means (31) for supplying cold gaseous fluid.
A device for crystallization of a component from a liquid mixture comprising an elongated chamber (1) having an upper part an intermediate part and a lower part said upper part having means (46) for supplying said liquid mixture, said intermediate part having collecting means (20) for, for withdrawing a suspension of crystals of the component in a mother liquor, and said lower part having means for separation and purification of resultant crystals, means (9) for supplying a cold gaseous fluid into at least one point located below the upper part of the elongated chamber and means (22) located in the upper part of the chamber for drawing off hot gaseous fluid resulting from direct countercurrent heat exchange of the cold gaseous fluid with aid liquid mixture, said device also comprising means for shaping a descending flow of the liquid mixture such that the cold gaseous fluid that circulates upward exchanges cold directly with the mixture that is shaped, wherein means (22) for drawing off the hot gaseous fluid are connected to at least one means (24b) for recompression of said hot gaseous fluid, wherein the recompression means has an output connected to at least one heat exchanger (27), wherein the heat exchanger has an output that is connected to a turbo-expander (30), and wherein the turbo-expander has an output connected to means (31) for supplying cold gaseous fluid.
Dependencies are inferred from the claim text.