Method of producing crystalline D-sorbitol
AssigneeMetallgesellschaft Aktiengesellschaft
InventorsPedro Gutmann, Jakob Wiesenbart
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AssigneeMetallgesellschaft Aktiengesellschaft
InventorsPedro Gutmann, Jakob Wiesenbart
Estimating the term…
The continuous process for making crystalline D-sorbitol using a melt crystallizer consisting of a cooled container and a horizontally arranged rotatable shaft equipped with disk elements and mixing parts to form a worm includes evaporating an aqueous D-sorbitol solution at 5 to 200 mbar and at a temperature of 130.degree. to 170.degree. C. in vacuum, advantageously in a thin film evaporator, to obtain a D-sorbitol melt containing less than 0.5 % by weight water; cooling the D-sorbitol melt to a temperature of 5 to 15.degree. C. above a solidification point of the D-sorbitol melt; melt crystallizing the D-sorbitol melt obtained during the evaporating in the melt crystallizer with an average dwell time of 1 to 5 hours to form D-sorbitol crystals and grinding and sieving the D-sorbitol crystals formed during the melt crystallizing of step d) to form a D-sorbitol end product containing more than 90% by weight of a .gamma. modification of crystalline D-sorbitol. During the process no solid D-sorbitol is added to the D-sorbitol melt in order to form initial crystallization nuclei for crystallization and no subsequent maturation steps of the end product are included in the process.
A continuous process for making crystalline D-sorbitol, said process comprising the steps of:
Dependencies are inferred from the claim text.