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US 6,110,620 AGranted
Controlled crystallite size electrode
AssigneeEveready Battery Company, Inc.
InventorsDeepika B. Singh, Jon R. Young
Life of this patent
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Abstract
This invention relates to methods for forming nickel hydroxide battery electrodes comprising nickel hydroxide particles which have crystallite sizes falling within the range of about 60 .ANG. to about 160 .ANG..
Claims34
A sintered electrode comprising Ni(OH).sub.2 particles in which all crystallites thereof fall within a size range of about 60 .ANG. to about 160 .ANG..
A method for producing a controlled crystallite size nickel hydroxide sintered electrode, having Ni(OH).sub.2 particles in which all crystallites thereof fall within a 60-160 .ANG. size range, comprising the steps of:
- providing a conductive metal sintered plaque substrate;
- and
- putting said substrate through at least one impregnation-cleaning series, said impregnation-cleaning series comprising the substeps of:
- a) impregnating said substrate with nickel hydroxide by putting said substrate through one or more impregnation cycles to form an impregnated substrate;
- and
- b) electrochemically cleaning said impregnated substrate at least once, said substep of electrochemically cleaning said impregnated substrate comprising the sub-substeps of:
- i) immersing said impregnated substrate into a solution of at least one caustic base, and
- ii) applying a charge to said impregnated substrate, said charge being equivalent to at least about 120% of single-electron capacity, but less than that producing crystallites less than about 60 .ANG. in size.
5 more elements
Dependencies are inferred from the claim text.