Process for making carbon foam
AssigneeLockheed Martin Engery Research Corporation
InventorJames W. Klett
Life of this patent
Estimating the term…
Abstract
The process obviates the need for conventional oxidative stabilization. The process employs mesophase or isotropic pitch and a simplified process using a single mold. The foam has a relatively uniform distribution of pore sizes and a highly aligned graphic structure in the struts. The foam material can be made into a composite which is useful in high temperature sandwich panels for both thermal and structural applications.
Claims38
A process of producing carbon foam comprising:
- selecting an appropriate mold shape;
- introducing pitch to an appropriate level in a mold;
- purging air from the mold;
- heating the pitch to a temperature sufficient to coalesce the pitch into a liquid;
- applying an inert fluid at a static pressure up to about 1000 psi;
- heating the pitch to a temperature sufficient to cause gases to evolve and foam the pitch;
- heating the pitch to a temperature sufficient to coke the pitch;
- and
- cooling the foam to room temperature with a simultaneous release of pressure to produce a carbon foam.
A process of producing carbon foam comprising:
- selecting an appropriate mold shape and a mold composed of
- a material that the molten pitch does not wet;
- introducing pitch to an appropriate level in the mold;
- purging the air from the mold;
- heating the pitch to a temperature sufficient to coalesce the pitch into a liquid;
- applying an inert fluid at a static pressure up to about 1000 psi;
- heating the pitch to a temperature sufficient to coke the pitch;
- and
- cooling the foam to room temperature with a simultaneous release of pressure to produce a carbon foam.
A process of producing carbon foam core composite comprising:
- selecting an appropriate mold shape;
- introducing pitch to an appropriate level in a mold;
- purging air from the mold;
- heating the pitch to a temperature sufficient to coalesce the pitch into a liquid;
- applying an inert fluid at a static pressure up to above 1000 psi;
- heating the pitch to a temperature sufficient to cause gases to evolve and foam the pitch;
- heating the pitch to a temperature sufficient to coke the pitch;
- cooling the foam to room temperature with a simultaneous release of pressure;
- placing facesheets on the opposite sides of the carbon foam;
- and
- adhering the facesheets to the carbon foam to produce a carbon foam core.
A process for producing a carbon foam comprising:
- providing pitch in a container;
- heating said pitch in a non-oxidizing atmosphere at a pressure and temperature sufficient to coalesce said pitch to form a liquid of said pitch;
- increasing said pressure of said non-oxidizing atmosphere in said container containing said liquid of said pitch from said pressure to an increased pressure having a range greater than said pressure to about 1000 psi;
- and
- heating said container containing said liquid of said pitch at said increased pressure to a temperature sufficient to form a carbon foam.
A process for producing a thermally conductive essentially graphitic carbon foam comprising:
- providing pitch in a container;
- heating said pitch in a non-oxidizing atmosphere at a pressure to a temperature sufficient to coalesce said pitch to form a liquid of said pitch;
- increasing said pressure of said non-oxidizing atmosphere in said container containing said liquid of said pitch from said pressure to an increased pressure having a range greater than said pressure to about 1000 psi;
- heating said container containing said liquid of said pitch at said increased pressure to a temperature sufficient to form a carbon form;
- cooling said carbon foam and reducing said increased pressure to atmospheric pressure;
- heating said carbon foam in a non-oxidizing atmosphere to a temperature sufficient to carbonize said carbon foam to form a carbonized carbon foam;
- and
- heating said carbonized carbon foam in a non-oxidizing atmosphere to a temperature sufficient to form a thermally conductive essentially graphitic carbon foam.
Dependencies are inferred from the claim text.