# US 5,916,084 A · Batch centrifuge for a mixture of solid and liquid and skim from molten aluminous metal

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- Number: US 5,916,084 A
- Document ID: US5916084A
- Status: Granted
- Kind: A
- Application number: 08/610,633
- Filed: 1996-03-04
- Granted: 1999-06-29
- Earliest claimed: 1996-03-04
- Assignees: Singleton Technology, Inc.
- Inventors: Ogle Ridout Singleton, Jr.
- Web page: https://patentgrep.com/patent/US5916084A

## CPC

- C22B 21/066: {Treatment of circulating aluminium, e.g. by filtration (C22B21/068 takes precedence)}
- B04B 9/14: Balancing rotary bowls (balancing per se G01M); {Schrappers}
- C22B 9/02: Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action {including acoustic waves; (C22B9/003, C22B9/006, C22B9/05, C22B9/22 take precedence)}
- Y02P 10/20: Recycling
- C22B: PRODUCTION AND REFINING OF METALS (electrolytic C25); PRETREATMENT OF RAW MATERIALS
- B04B: CENTRIFUGES (high-speed drum mills B02C19/11; domestic spin driers D06F; analysing, measuring or monitoring physical or chemical properties of samples during centrifuging, see the relevant subclasses for these procedures, e.g. G01N)
- Y02P: CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS

## Abstract

A suspended centrifuge apparatus has been improved by the addition of a restraint that closely maintains the original, static, vertical axis of a suspended centrifuge vessel during rotation. The restraint is preferably located to act on the lower half of the suspended vessel and preferably limits axial gyration to less than 5-degrees. A further improvement is a centrifuge bowl configuration which provides a protected surface to be acted on by a gyration restraint while partially eliminating centrifuge bowl capacity in a lower, central region subjected to inherently low centrifugal forces. An improved liquid separation process results from the use of the improved apparatus to better control the liquid discharge trajectory from the rotating centrifuge. Process control and safety are also improved.

## Claims

### Claim 1

A suspended centrifuge apparatus for the removal of liquid from a physical mixture of at least one liquid phase and at least one particulate solid phase, said physical mixture including, inter alia, hot aluminous skim having a liquid aluminum component, said suspended centrifuge apparatus comprising:
a centrifuge vessel;
a structural support comprising a means for suspending, for positioning and for rotating a first, compound, arcuate surfaced, linkage component, enabling suspension, positioning and rotation of said centrifuge vessel;
a second, arcuate surfaced, linkage component mountably and demountably engageable with the first linkage component, having a central axis and attached to said centrifuge vessel;
said first linkage component and the second linkage component, when fully engaged, forming a linkage interconnection point;
said centrifuge vessel comprising: at least one peripheral opening of controlled extent, a vertical, central axis, said vessel being generally symmetrical about said vertical, central axis, and having walls and a closed bottom with an indentation therein, and
said central axis of said second linkage component capable of being located coextensive with said vertical, central axis of said centrifuge vessel;
said centrifuge vessel when loaded, suspended from said structural support and, prior to rotation, assuming an initial, static, vertical axis as measured from said linkage interconnection point;
said indentation defining a generally conical, rigid, exterior surface of said centrifuge vessel and having a central axis coextensive with said vertical, central axis of said centrifuge vessel, the bottom diameter of said indentation being greater than the upper diameter of said indentation;
a first, centrifuge vessel, gyration restraint component being a portion of said generally conical, rigid, exterior surface of said indentation on the exterior of said centrifuge vessel;
a second, centrifuge vessel, gyration restraint component being fixed in space and comprising: an exterior surface able to cooperate with a portion of said first, centrifuge vessel, gyration restraint component and having an upper, exterior portion smaller by a predetermined amount than a lower, exterior portion of said first, centrifuge vessel, gyration restraint component; and
during liquid extraction, said suspended centrifuge vessel being positioned with said first, centrifuge vessel, gyration restraint component surrounding proximate a predetermined distance from the cooperating portion of said second, centrifuge vessel, gyration restraint component, thereby enabling, during centrifuging, said vertical, central axis of said centrifuge vessel to be maintained closely to said initial, static, vertical axis measured from said linkage interconnection point;
whereby, the loaded, suspended, and positioned centrifuge vessel is enabled by a predetermined speed and time of rotation under gyration restraint to expel most of said at least one liquid phase and retain most of said at least one particulate solid phase thereby effectively separating said physical mixture.

### Claim 2 (depends on 1)

The suspended centrifuge apparatus of claim 1 further comprising: a liquid collecting means disposed around and spaced a predetermined distance from said second centrifuge vessel gyration restraint component and, at the same time, disposed with predetermined spatial clearance around said centrifuge vessel when said centrifuge vessel is positioned for rotation and when rotating, so that said liquid collecting means is capable of receiving material expelled from said at least one peripheral opening of said centrifuge vessel.

### Claim 3 (depends on 1)

The suspended centrifuge apparatus of claim 1 wherein said centrifuge vessel comprises: a bowl, a detachable bowl cover with means to lock said detachable cover to said bowl.

### Claim 4 (depends on 3)

The suspended centrifuge apparatus of claim 3 wherein said second, arcuate surfaced, linkage component is mounted to said detachable bowl cover.

### Claim 5 (depends on 1)

The suspended centrifuge apparatus of claim 1 wherein at least one element of said second, centrifuge vessel, gyration, restraint component is rotatable about a fixed axis.

### Claim 6 (depends on 1)

The suspended centrifuge apparatus of claim 1 wherein said predetermined distance of said exterior cooperating portion of said second, centrifuge vessel, gyratory restraint component is positioned from said first, centrifuge vessel, gyratory restraint component during centrifuging such that said central, vertical axis of said centrifuge vessel is limited to a gyration of not more than about five degrees from the initial, static, vertical axis of said centrifuge vessel as measured from said linkage interconnection point.

### Claim 7 (depends on 1)

The suspended centrifuge apparatus of claim 1 wherein said structural support is positionable.

### Claim 8 (depends on 1)

The suspended centrifuge apparatus of claim 1 whereby said suspended centrifuge apparatus separates at least a portion of said liquid aluminum component from said hot aluminous skim.

### Claim 9

A suspended centrifuge apparatus for the separation of a physical mixture of at least one liquid phase and at least one solid particulate phase into a retained, enriched in solids residue and an expelled liquid enriched phase, said physical mixture including hot aluminous skim having a liquid aluminum metal component said suspended centrifuge apparatus comprising:
a centrifuge vessel;
a structural support comprising a means for suspending, for positioning and for rotating a first linkage member having a compound arcuate linking surface and enabling suspension, positioning and rotation of said centrifuge vessel;
said centrifuge vessel comprising: a bowl and a second linkage member having an arcuate linking surface mountably and demountably engageable with said first linkage member;
said bowl having a central, vertical axis and said second linkage member having a vertical, central axis coextensive with said central, vertical axis of said bowl,
said bowl being generally symmetrical, inside and out about said central, vertical axis and having a rigid side wall connected to a bottom wall,
said bowl capable of holding and transporting a predetermined quantity of said physical mixture and holding and transporting said retained, enriched in solids residue,
said bowl having on a lower portion of said rigid side wall, an exterior surface being a surface of revolution selected from the group comprising a cylinder and a cone, said lower portion of said rigid side wall exterior surface being a first gyratory restraint member;
said centrifuge vessel having at least one peripheral opening;
said first linkage member and said second linkage member when fully engaged forming a linkage interconnection point;
said centrifuge vessel, when loaded, suspended from said first linkage member and prior to rotation assuming an initial static vertical axis as measured from said linkage interconnection point;
a second gyratory restraint member, fixed in space comprising:
a means to cooperate with said first gyratory restraint member so that, when the loaded, suspended centrifuge vessel is positioned with said first gyratory restraint member in a predetermined, cooperative relationship with said second gyratory restraint member, said second gyratory restraint member provides a guideway within which a substantial portion of said first gyration restraint member can freely rotate and with said guideway limiting the gyratory motion of said central vertical axis of said centrifuge vessel closely to said initial, static, vertical axis of said centrifuge vessel as measured from said linkage interconnection point;
whereby, said loaded, suspended centrifuge vessel is enabled, by a predetermined speed and time of rotation and under gyratory restraint, to expel most of said at least one liquid phase and retain most of said at least one solid particulate phase; thereby, effectively separating said physical mixture.

### Claim 10 (depends on 9)

The suspended centrifuge apparatus of claim 9 with the addition of a liquid collecting means, disposed proximate to said second gyratory restraint member and surrounding by a predetermined distance and extent from said centrifuge vessel when said centrifuge vessel is positioned for liquid extraction so that, during rotation, expelled material is intercepted and collected.

### Claim 11 (depends on 10)

The suspended centrifuge apparatus of claim 10 wherein said predetermined, cooperative relationship between said first and second gyratory restraint members is such that the gyration of said centrifuge vessel during rotation is restrained so that clearance is maintained between said centrifuge vessel and said liquid collecting means.

### Claim 12 (depends on 10)

The suspended centrifuge apparatus of claim 10 whereby said suspended centrifuge apparatus separates at least a portion of said liquid aluminum metal from said hot aluminous skim.

### Claim 13 (depends on 9)

The suspended centrifuge apparatus of claim 9 wherein said centrifuge vessel comprises: said bowl, a detachable bowl cover with means to lock said detachable bowl cover to said bowl.

### Claim 14 (depends on 9)

The suspended centrifuge apparatus of claim 9 wherein said second gyratory restraint member has at least one component rotatable about a fixed axis which can contact and guide said first gyratory restraint member during rotation of said centrifuge vessel.

### Claim 15 (depends on 9)

The suspended centrifuge apparatus of claim 9 wherein said predetermined, cooperative relationship between said first and second gyratory restraint members is such that the gyration of said central, vertical axis of said centrifuge bowl during rotation of said centrifuge vessel does not exceed about five degrees as measured from the linkage interconnection point.

### Claim 16 (depends on 9)

The suspended centrifuge apparatus of claim 9 wherein said structural support is positionable.

### Claim 17 (depends on 9)

The suspended centrifuge apparatus of claim 9 whereby said suspended centrifuge apparatus separates at least a portion of said liquid aluminum metal from said hot aluminous skim.

### Claim 18 (depends on 9)

The suspended centrifuge apparatus of claim 9 whereby said suspended centrifuge apparatus separates at least a portion of said at least one liquid phase from said at least one solid particulate phase.