US 5,861,949 AGranted

Atomic absorption spectrophotometer

AssigneeShimadzu Corporation

InventorSeiji Kojima

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Abstract

Turning on a hollow cathode lamp of an objective element, the intensity of the light is measured while scanning the wavelength within a predetermined range centering around the resonance line of the objective element by rotating a diffraction grating by a pulse motor. Then a spectrum is constructed on the screen of a display unit within the above range, and the user operates an operation unit to point out the peak of the resonance line in the spectrum. The number of the driving pulses sent to the pulse motor when the pointed peak is detected is saved in an EEPROM so that the number corresponds to the wavelength of the resonance line. After that, when the objective element in a sample is measured, the above number is read out from the EEPROM and the pulse signals are sent to the pulse motor by the number, whereby the diffraction grating is set at an angular position corresponding to the resonance line of the element correctly.

Claims5

Dependent claims

An atomic absorption spectrophotometer for analyzing a sample by a process including steps of passing a light generated by a light source through an atomized sample, extracting a monochromatic light having a predetermined wavelength with a monochromator including a dispersing device and detecting the extracted light by a photodetector, comprising:

a) driving means for changing the orientation of the dispersing device;
b) first memory means for storing data of a relation between the wavelength of the monochromatic light produced with the monochromator and a controlling input of the driving means;
c) control means for varying the controlling input of the driving means based on the data of the relation stored in the first memory means, so that the wavelength is scanned within a predetermined proximity to a wavelength of a resonance line of an objective element, using a light source of the objective element before an analysis of the sample is started;
d) displaying means for displaying a distribution of the intensity of light detected by the photodetector while the wavelength is scanned;
e) pointing means for a user to point out a peak corresponding to the objective element in the distribution of the intensity of light displayed on a display unit;
and
f) second memory means for storing data of the controlling input of the driving means at the peak position so that the data corresponds to the wavelength of the resonance line of the objective element.

4 more elements

Dependencies are inferred from the claim text.