Apparatus and process for a polycondensation reaction
AssigneeE. I. Du Pont de Nemours and Company
InventorKamlesh Kumar Bhatia
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AssigneeE. I. Du Pont de Nemours and Company
InventorKamlesh Kumar Bhatia
Estimating the term…
An improved process and apparatus for the production of a polyester or other condensation polymer is disclosed. In particular, polymerization is conducted in a reaction vessel equipped with a specially designed agitator that exposes the polymer melt partially filling the reaction vessel to inert gas flowing through the vessel. The agitator comprises a plurality of elements that lift a portion of a polymer melt in the reaction vessel and generate films of the polymer melt which films extends in planes that are parallel to the axis of the agitator and the flow of gas through the reaction vessel. In a preferred process, a melt of bis(2-hydroxyethyl) terephthalate, or its low molecular oligomers, obtained by esterifying terephthalic acid or transesterifying dimethyl terephthalate with ethylene glycol, is contacted with an inert gas at about atmospheric pressure in order to remove the reaction by-products and facilitate polymerization.
A process for manufacturing a polyester of one or more aromatic dicarboxylic acids and one or more glycols in a molten state in which an inert gas is employed to assist in removing a volatile condensation by-product, wherein the improvement comprises, employing a horizontally disposed cylindrical reactor vessel partly filled with a polymerization reaction mass in the form of a melt, which reactor vessel is equipped with the following:
An apparatus for conducting a condensation polymerization in a molten state, which apparatus comprises a horizontally disposed cylindrical reactor equipped with the following:
Dependencies are inferred from the claim text.