# US 5,733,390 A · Carbon-titanium composites

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- Number: US 5,733,390 A
- Document ID: US5733390A
- Status: Granted
- Kind: A
- Application number: 08/568,530
- Filed: 1995-12-07
- Granted: 1998-03-31
- Earliest claimed: 1993-10-18
- Assignees: Ticomp, Inc.
- Inventors: William R. Kingston
- Web page: https://patentgrep.com/patent/US5733390A

## CPC

- B32B 15/08: of synthetic resin
- B32B 38/0036: {Heat treatment (for heating or cooling of layers during lamination B32B37/06, B32B37/08)}
- A63B 59/50: Substantially rod-shaped bats for hitting a ball in the air, e.g. for baseball
- A63B 2102/18: Baseball, rounders or similar games
- A63B 2209/02: with reinforcing fibres, e.g. carbon, polyamide fibres
- B32B 2038/0016: {Abrading}
- B32B 2038/0076: {Curing, vulcanising, cross-linking}
- B32B 2305/08: Reinforcements
- B32B 2311/00: Metals, their alloys or their compounds
- B32B: LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- A63B: APPARATUS FOR PHYSICAL TRAINING, GYMNASTICS, SWIMMING, CLIMBING, OR FENCING; BALL GAMES; TRAINING EQUIPMENT (apparatus for passive exercising, massage A61H)

## Abstract

A method of combining a beta titanium alloy with advanced carbon composites, the combination having a matched yield strength and modules of elasticity ratio. When the combination is adhesively bonded both parts will approach maximum yield strength and fail at a similar amount of total strain. The titanium and carbon composites are combined by first abrading the titanium to be bonded, coating the titanium with platinum, aging the titanium, spraying primer on the coated titanium, applying adhesive to the primer side of the titanium and then applying the carbon to the adhesive. This allows the carbon composite to bond securely to the titanium. This composite uses the best properties of each component, the combination having a better set of properties than either part.

## Claims

### Claim 1

A method of preparing a carbon-titanium composite comprising the steps of:
(a) providing a beta titanium alloy having a surface with an area;
(b) coating the surface of the beta titanium alloy with a metal selected from the group consisting of platinum and the functional equivalent of platinum as a coating material, to produce a coated titanium alloy;
(c) heating the coated beta titanium alloy at a temperature for a time to produce an aged coated beta titanium alloy; and
(d) adhering a carbon composite having a strength to modulus of elasticity ratio to the aged coated beta titanium alloy;
wherein the heating step imparts to the coated beta titanium alloy a yield strength to modulus of elasticity ratio that is substantially similar to the strength to modulus of elasticity ratio of the carbon composite.

### Claim 2 (depends on 1)

The method of claim 1, additionally comprising the step of abrading the surface of the beta titanium alloy to increase the area of the surface after step (a).

### Claim 3 (depends on 1)

The method of claim 1, additionally comprising the step of priming the aged surface with a primer after step (c).

### Claim 4 (depends on 1)

The method of claim 1, wherein the adhering step, step (d), comprises applying an adhesive to the aged coated beta titanium alloy.

### Claim 5 (depends on 4)

The method of claim 4, additionally comprising the step of bonding the carbon composite to the adhesive by heating the carbon composite.

### Claim 6 (depends on 1)

The method of claim 1, wherein the beta titanium alloy is selected from the group consisting of (Ti--15V--3Cr--3Sn--3Al) and (Ti--15Mo--3Al--3Nb).

### Claim 7 (depends on 1)

The method of claim 1, wherein the temperature of step (c) is approximately 950.degree. F. and the time of step (c) is approximately 8 hours.

### Claim 8 (depends on 1)

A method of making an airplane part, comprising the steps of:
(a) preparing a carbon-titanium composite according to the method of claim 1; and
(b) incorporating the carbon-titanium composite into an airplane part.

### Claim 9 (depends on 8)

The method of making an airplane part of claim 8, wherein the airplane part of step (b) is selected from the group consisting of airplane skin, a hat section stiffener, a plate and a tube.

### Claim 10 (depends on 8)

A method of making an airplane, comprising the steps of:
(a) preparing an airplane part according to the method of claim 8; and
(b) incorporating the part into an airplane.

### Claim 11 (depends on 1)

A method of making an airplane, comprising the steps of:
(a) providing a carbon-titanium composite according to the method of claim 1;
(b) utilizing the carbon-titanium composite to produce an airplane part; and
(c) incorporating the part into an airplane part.

### Claim 12 (depends on 11)

The method of making an airplane of claim 11, wherein the airplane part of step (b) is selected from the group consisting of airplane skin, a hat section stiffener, a plate and a tube.