# US 5,708,219 A · Multisample dynamic headspace sampler

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- Number: US 5,708,219 A
- Document ID: US5708219A
- Status: Granted
- Kind: A
- Application number: 08/780,883
- Filed: 1997-01-09
- Granted: 1998-01-13
- Earliest claimed: 1995-09-12
- Assignees: Seagate Technology LLC
- Inventors: Karl H. Scheppers; Gregory I. Rudd
- Web page: https://patentgrep.com/patent/US5708219A

## CPC

- G01N 1/26: with provision for intake from several spaces
- G01N 1/2214: {by sorption}
- G01N 1/405: {by adsorption or absorption}
- G01N 7/14: by allowing the material to emit a gas or vapour, e.g. water vapour, and measuring a pressure or volume difference {(determining urea G01N33/48742)}
- G01N 2001/2229: {Headspace sampling, i.e. vapour over liquid}
- G01N 2035/00356: {Holding samples at elevated temperature (incubation)}
- Y10T 137/87877: Single inlet with multiple distinctly valved outlets
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- Y10T: TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION

## Abstract

Method and apparatus for collecting a large number of outgas samples at the same time. Specimens to be tested for outgassing are placed in throw-away widemouth bottles, and the bottles are placed in cups provide in a heating block. A custom made cap is fastened to each bottle using an O-ring. Each cap is provided with an outgassing sample collecting tube. A source of pure gas such as nitrogen or helium is connected by way of a pressure regulator and a hydrocarbon filter to a manifold. Each of the caps on each bottle is coupled to the manifold by way of a metering valve. An adsorbent is placed in each collecting tube. The gas pressure is set to between 10 and 15 psi. The flow through each collecting tube is set to a predetermined level by adjusting its metering valve and measuring the flow at the exit of the collecting tube using a flowmeter. The healing block is heated by means of a thermal tape used in conjunction with a power supply and a thermocouple inserted into a hole in the heating block. The samples are heated and held at an elevated temperature for a predetermined length of time. After the outgassing test is completed, the collecting tubes are desorbed and analyzed with the appropriate instrumentation.

## Claims

### Claim 1

A manifold for a multichamber dynamic headspace sampler comprising:
an elongated tube, each end of said tube being threaded, the wall of said tube being provided with a plurality of threaded holes along the length thereof in diametrically opposite pairs,
two pipe end caps, one cap for each end of said tube, one of said caps being provided with an opening through one end thereof, said opening being adapted to be coupled to a source of compressed gas;
a plurality of metering valves, each individually connected to one of said threaded holes;
said plurality of metering valves being adapted to couple to sample chambers disposed in a heater block for providing compressed gas thereto.

### Claim 2

A manifold for an outgas test fixture for simultaneously sampling off-gassed organic compounds from a plurality of specimens in a plurality of sample chambers disposed in a heater block, said manifold comprising:
an elongated pipe provided with a plurality of threaded holes;
two pipe caps, one provided at each end of said elongated pipe;
a connector disposed in one of said pipe caps, said connector being adapted to be coupled to a source of compressed gas;
a plurality of metering valves, each individually connected to one of said threaded holes;
a plurality of port connectors, each individually connected to one said metering valves;
a plurality of tubing unions, each individually connected to one of said port connectors;
a plurality of flexible tubes, each individually connected to one of said tubing unions; and
a plurality of O-ring adapters, each individually connected to one of said flexible tubes, said O-ring adapters being adapted to couple to sample chambers disposed in a heater block.

### Claim 3

A manifold for an outgas test fixture for simultaneously sampling off-gassed organic compounds from a plurality of specimens in a plurality of sample chambers disposed in a heater block, said manifold comprising:
a stainless steel pipe 1/2 inch in diameter and 17 inches long provided with twelve threaded holes, six holes along each side thereof, said twelve threaded holes having a 1/8-27 NPT thread;
two pipe caps, one provided at each end of said stainless steel pipe;
a connector disposed in one of said pipe caps, said connector being adapted to be coupled to a source of compressed gas;
twelve metering valves, each individually connected to one of said twelve threaded holes;
twelve port connectors, each individually connected to one said twelve metering valves;
twelve tubing unions, each individually connected to one of said twelve port connectors;
twelve stainless steel flexible tubes, each individually connected to one of said twelve tubing unions; and
twelve O-ring adapters, each individually connected to one of said twelve stainless steel flexible tubes, said twelve O-ring adapters being adapted to couple to sample chambers disposed in a heater block.