# US 5,708,191 A · Ultrasonic fluid densitometry and densitometer

> Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt

- Number: US 5,708,191 A
- Document ID: US5708191A
- Status: Granted
- Kind: A
- Application number: 08/628,834
- Filed: 1996-04-05
- Granted: 1998-01-13
- Earliest claimed: 1996-04-05
- Assignees: Battelle Memorial Institute
- Inventors: Margaret S. Greenwood; Jason C. Lail
- Web page: https://patentgrep.com/patent/US5708191A

## CPC

- G01N 29/223: {Supports, positioning or alignment in fixed situation (mounting transducers per se G10K11/004)}
- G01N 9/002: {using variation of the resonant frequency of an element vibrating in contact with the material submitted to analysis (G01N9/34 takes precedence)}
- G01N 29/032: by measuring attenuation of acoustic waves
- G01N 2291/018: Impedance
- G01N 2291/02809: Concentration of a compound, e.g. measured by a surface mass change
- G01N 2291/02818: Density, viscosity
- G01N 2291/045: External reflections, e.g. on reflectors
- G01N 2291/105: two or more emitters, two or more receivers
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

The present invention is an ultrasonic fluid densitometer that uses a material wedge having an acoustic impedance that is near the acoustic impedance of the fluid, specifically less than a factor of 11 greater than the acoustic impedance of the fluid. The invention also includes a wedge having at least two transducers for transmitting and receiving ultrasonic signals internally reflected within the material wedge. Density of a fluid is determined by immersing the wedge into the fluid and measuring reflection of ultrasound at the wedge-fluid interface.

## Claims

### Claim 1

An ultrasonic densitometer for measuring a density of a fluid, said ultrasonic densitometer having at least one wedge material, said at least one wedge material having at least two sides substantially parallel, a first parallel side having a first ultrasonic transducer mounted thereon and a second parallel side immersible into said fluid whereby an ultrasonic signal emanating from said first ultrasonic transducer strikes said second parallel side and reflects back to said first parallel side; the improvement comprising:
(a) a first non-parallel side from which emanates a second reflected ultrasonic signal toward a second non-parallel side; and
(b) a receiving ultrasonic transducer mounted on said second non-parallel side for receiving said second reflected ultrasonic signal.

### Claim 2 (depends on 1)

The ultrasonic densitometer as recited in claim 1, wherein each of said first and second non-parallel sides is connected to said first and second parallel sides.

### Claim 3 (depends on 2)

The ultrasonic densitometer as recited in claim 2, further comprising:
a transmitting transducer mounted on said first non-parallel side whereby said transmitting transducer transmits said second ultrasonic signal that reflects from said second parallel side creating said second reflected ultrasonic signal that is received by said receiving transducer.

### Claim 4 (depends on 1)

The ultrasonic densitometer as recited in claim 1, wherein said first non-parallel side is a cut in said second parallel side and said second non-parallel side is connected to said first and second parallel sides, whereby an ultrasonic signal transmitted by said first transducer is reflected by both the second parallel side and said first non-parallel side producing a reflected signal from said second parallel side to the first transducer and producing said second reflected signal from said first non-parallel side to said receiving transducer.

### Claim 5 (depends on 1)

The ultrasonic densitometer as recited in claim 1, wherein said at least one wedge material is a plastic and said fluid has an aqueous phase.

### Claim 6 (depends on 1)

The ultrasonic densitometer as recited in claim 1, further comprising:
(a) a transmitting ultrasonic transducer mounted on said first non-parallel side that emits a second ultrasonic signal that reflects from said second parallel side thereby creating said second reflected ultrasonic signal, said first and second non-parallel sides making a first angle with said first parallel side; and
(b) a third non-parallel side having a second transmitting ultrasonic transducer that emits a third ultrasonic signal that reflects from said second parallel side and creating a third reflected ultrasonic signal that is received by a second receiving ultrasonic transducer mounted on a fourth non-parallel side, said third and fourth non-parallel sides making a second angle with said first parallel side different from said first angle.

### Claim 7 (depends on 6)

The ultrasonic densitometer as recited in claim 6, further comprising:
a fourth transmitting ultrasonic shear wave transducer mounted on said first parallel side.

### Claim 8 (depends on 1)

The ultrasonic densitometer as recited in claim 1, wherein said second non-parallel side forms an angle with said second parallel side, said angle at least 20 degrees.

### Claim 9 (depends on 8)

The ultrasonic densitometer as recited in claim 8, wherein said angle is 60 degrees.

### Claim 10 (depends on 1)

The ultrasonic densitometer as recited in claim 1, wherein said first and second non-parallel sides are on a first wedge and said first and second parallel sides are on a second wedge.

### Claim 11

A method of measuring density of a fluid ultrasonically, comprising the steps of:
(a) providing at least one wedge material, said at least one wedge material having at least two sides substantially parallel, mounting a first ultrasonic transducer on a first parallel side and immersing a second parallel side into said fluid and emanating an ultrasonic signal from said first ultrasonic transducer, said ultrasonic signal striking said second parallel side and reflecting back to said first parallel side; wherein the improvement comprises:
(b) emanating a second reflected ultrasonic signal from a first non-parallel side toward a second non-parallel side; and
(c) receiving said second reflected ultrasonic signal with a receiving ultrasonic transducer on said second non-parallel side.

### Claim 12 (depends on 11)

The method as recited in claim 11, wherein each of said first and second non-parallel sides is connected to said first and second parallel sides.

### Claim 13 (depends on 11)

The method as recited in claim 11, wherein said first and second non-parallel sides are on a first wedge and said first and second parallel sides are on a second wedge.

### Claim 14 (depends on 11)

The method as recited in claim 11, wherein said second non-parallel side forms an angle with said second parallel side, said angle at least 20 degrees.

### Claim 15 (depends on 14)

The method as recited in claim 14, wherein said angle is 60 degrees.
