# US 5,707,592 A · Method and apparatus for treatment of waste materials including nuclear contaminated materials

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- Number: US 5,707,592 A
- Document ID: US5707592A
- Status: Granted
- Kind: A
- Application number: 08/538,502
- Filed: 1995-09-29
- Granted: 1998-01-13
- Earliest claimed: 1991-07-18
- Inventors: Edward Someus
- Web page: https://patentgrep.com/patent/US5707592A

## CPC

- G21F 9/32: by incineration
- G21F 9/301: {by fixation in stable solid media}
- G21F 9/304: {Cement or cement-like matrix (compositional aspects C04B)}
- G21F: PROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR (radiation protection by pharmaceutical means A61K8/00, A61Q17/04; in cosmonautic vehicles B64G1/54; combined with a reactor G21C11/00; combined with X-ray tubes H01J35/16; combined with X-ray apparatus H05G1/02)

## Abstract

A method and apparatus for the treatment of waste materials including nuclear contaminated materials is disclosed. The method of the invention includes the steps of: grinding the base material until the maximum grain size is 50 millimeters; drying the ground material to a relative humidity content below 30%; distilling the material at a core temperature of 100.degree.-1200.degree. C. on a negative pressure from 200 N/m.sup.2 to an over pressure of 300 kN/m.sup.2 in an oxygen free, reducing, indirect heated environment; burning or cooling the vapors arising; treating the remaining solid materials by combustion, mineralization, vitrification, or solidification; and pelletizing or granulating the remaining ash. The apparatus of the invention includes a dry distillation reactor that has a rotary, closed, horizontally arranged cylinder with hollow axes on the ends. The axes are separated from input and output houses by seals. The input house is provided with a loading opening and a gas exit branch. The output house is provided with an unloading opening and a gas exit branch. The ends are sealed by sealing segments placed on the axes and sealing rings placed between the sealing segments and the walls of the input and output house.

## Claims

### Claim 1

A reactor for the treatment of waste materials comprising:
a rotary, closed horizontally arranged cylinder, said cylinder having a first and a second end;
a pair of hollow axes, the first axes being placed on the first end of said cylinder and the second axes being placed on the second end of said cylinder;
two bearing means for supporting the first and second axes and for providing rotating movement;
an input house for introducing materials connected to the outer end of the first axes;
an output house connected to the outer end of the second axes;
a pair of sealing means, the first sealing means being placed on the first axes between the input house and the first end of the cylinder and the second sealing means being placed on the second axes between the output house and the second end of the cylinder; and
an input pulley built-in into the hollow of the sideways axis of the input house, wherein said input house has a loading opening and a gas exit branch, said output house has an unloading opening and a gas exit branch, and said cylinder is provided with carrying-out shovels fixed to the interior surface of the cylinder at the side of the output house.

### Claim 2 (depends on 1)

A reactor according to claim 1 wherein said sealing means comprises:
a plurality of sealing segments arranged circumferentially on the first and second axes;
a pair of sealing rings, the first sealing ring being placed between said sealing segments and the wall of the input house nearest the cylinder and the second sealing ring being placed between said sealing segments and the wall of the output house nearest the cylinder;
a cord for drawing together said sealing segments;
weights for pulling said cord;
holders fixed to the walls of the input and output house nearest the cylinder for securing the sealing rings against radial displacement; and
a clamping means for securing said sealing segments and said sealing rings against axial displacement.

### Claim 3 (depends on 1)

A reactor according to claim 1 wherein the waste materials are nuclear contaminated materials.
