# US 5,707,574 A · Method for the unilateral or bilateral sealing or filling of flow channels in an annular zone of a cylindrical honeycomb body

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- Number: US 5,707,574 A
- Document ID: US5707574A
- Status: Granted
- Kind: A
- Application number: 08/498,060
- Filed: 1995-07-05
- Granted: 1998-01-13
- Earliest claimed: 1994-07-08
- Assignees: Degussa AG
- Inventors: Rainer Domesle; Bernd Engler; Wolfgang Kuhl; Egbert Lox; Oliver Fehnle; Walter Leibold
- Web page: https://patentgrep.com/patent/US5707574A

## CPC

- B01J 37/00: Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS

## Abstract

A method for the sealing of flow channels in an annular zone of a cylindrical honeycomb body. The sealing of the flow channels takes place by introduction of a ceramic compound into the flow channels by means of a nozzle, wherein nozzle and honeycomb body are moved relative to one another with simultaneous guiding of the nozzle past the lateral surface and/or past the end face contour of the honeycomb body.

## Claims

### Claim 1

A method for the unilateral or bilateral sealing or filling of flow channels in an annular zone of a cylindrical honeycomb body which is bounded by two end faces having a contour, which form the inlet and outlet face of said honeycomb body, and by an enveloping lateral surface, comprising introducing a ceramic compound into said flow channels in said annular zone of at least one of said end faces by means of at least one nozzle having a nozzle opening, wherein the width of said nozzle opening is at least equal to the greatest diagonal of a flow channel and wherein the sealing or filling of said flow channels is performed by locating the nozzle over said end face and moving said nozzle and said end faces laterally relative to one another during sealing or filling of said flow channels with simultaneous guiding of said nozzle over said end face in said annular zone during said sealing or filling along said lateral surface or along said contour of said end face.

### Claim 2 (depends on 1)

The method according to claim 1, further comprising application of an over- or under-pressure onto said ceramic compound during said introducing or after completion of said introducing.

### Claim 3 (depends on 1)

The method according to claim 1, wherein said flow channels are sealed by introducing said ceramic compound up to a depth of 10 mm.

### Claim 4 (depends on 1)

The method according to claim 1, wherein said flow channels are filled by introducing said ceramic compound along the entire length of said honeycomb body.

### Claim 5 (depends on 1)

The method according to claim 1, wherein said flow channels are sealed by said inlet and outlet face successively or simultaneously.

### Claim 6 (depends on 1)

The method according to claim 1, wherein said flow channels of said annular zone are sealed or filled only in portions of said annular zone.

### Claim 7 (depends on 1)

The method according to claim 1, wherein said annular zone forms the edge zone of said honeycomb body.

### Claim 8 (depends on 1)

The method according to claim 1, wherein said ceramic compound introduced into said flow channels is dried by microwaves and optionally cured by calcination to form a cured ceramic compound.

### Claim 9 (depends on 8)

The method according to claim 8, wherein the coefficient of thermal expansion of said cured ceramic compound exceeds the coefficient of thermal expansion of said honeycomb body by not more than a factor of 5.

### Claim 10 (depends on 9)

The method according to claim 9, wherein said coefficient of thermal expansion of said cured ceramic compound exceeds said coefficient of thermal expansion of said honeycomb body by not more than a factor of 3.

### Claim 11 (depends on 1)

The method according to claim 1, wherein said nozzle is guided along past said lateral surface and/or past the contour of said end face or that said honeycomb body is rotated away about its axis below said nozzle.