# US 5,705,229 A · Process for producing composite material combining a magnesium alloy containing zirconium with a carbon reinforcement

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- Number: US 5,705,229 A
- Document ID: US5705229A
- Status: Granted
- Kind: A
- Application number: 08/639,195
- Filed: 1996-04-26
- Granted: 1998-01-06
- Earliest claimed: 1992-09-10
- Assignees: Aerospatiale Societe Nationale Industrielle
- Inventors: Henri Abiven; Lionel Picquet; Gilles Claveyrolas; Jean-Claude Viala; Jean Bouix
- Web page: https://patentgrep.com/patent/US5705229A

## CPC

- C22C 47/16: by thermal spraying of the metal, e.g. plasma spraying {(atomising molten metal comprising fibres see also C22C1/1042)}
- C22C 49/14: characterised by the fibres or filaments
- Y10T 428/12444: Embodying fibers interengaged or between layers [e.g., paper, etc.]
- Y10T 428/12486: Laterally noncoextensive components [e.g., embedded, etc.]
- C22C: ALLOYS (treatment of alloys C21D, C22F)
- Y10T: TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION

## Abstract

The invention relates to a composite material combining a magnesium alloy containing zirconium with a carbon reinforcement, as well as to its production process. According to the invention, such a composite material is prepared by the infiltration of a reinforcement formed from graphite or carbon fibres by a liquid magnesium alloy containing 0.3 to 1% by weight zirconium at a temperature of 650.degree. to 850.degree. C. Under these conditions, on said fibres is formed a zirconium carbide layer containing magnesium in solid solution and e.g. complying with the formula ZrC.sub.x Mg.sub.y with 0.3<x<1 and 0.02<y<0.12, which leads to the wetting of the fibres by the melted magnesium and to a good adhesion between the fibres and the matrix, without any deterioration to the mechanical characteristics of the fibres.

## Claims

### Claim 1

Process for the production of a composite material comprising a magnesium alloy matrix containing zirconium and a reinforcement of graphite or carbon fibres dispersed in said matrix and having a zirconium carbide layer containing magnesium in solid solution at the interface between the fibres and the magnesium-based matrix, which comprises infiltrating into said reinforcement a liquid magnesium alloy containing zirconium, the zirconium content said alloy being maintained at saturation during said infiltrating, said infiltration carried out at a temperature of 650.degree. to 850.degree. C. while maintaining said temperature for about 2-60 min.

### Claim 2 (depends on 1)

Process according to claim 1, characterized in that infiltration takes place by immersing a carbon or graphite fibre reinforcement in a molten magnesium alloy bath.

### Claim 3 (depends on 1)

Process according to claim 1, characterized in that infiltration takes place by hot compression of an alternating stack of carbon or graphite fibre reinforcements, magnesium alloy strips and zirconium powder.

### Claim 4 (depends on 1)

Process according to claim 1, characterized in that the magnesium alloy does not contain aluminium.