# US 5,705,225 A · Method of filling pores in anodized aluminum parts

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- Number: US 5,705,225 A
- Document ID: US5705225A
- Status: Granted
- Kind: A
- Application number: 08/619,263
- Filed: 1996-03-18
- Granted: 1998-01-06
- Earliest claimed: 1993-10-15
- Assignees: Applied Materials, Inc.
- Inventors: Charles Dornfest; Fred C. Redeker; Mark Anthony Fodor; Craig Bercaw; H. Steven Tomozawa
- Web page: https://patentgrep.com/patent/US5705225A

## CPC

- C25D 11/18: After-treatment, e.g. pore-sealing
- C25D: PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR

## Abstract

Anodized aluminum coatings employed in semiconductor processing equipment are treated to reduce their sensitivity to halogenated species. The pores of the aluminum oxide surface can be filled either by a metal, such as magnesium or aluminum, forming the corresponding metal oxide that is resistant to reaction with halogens, or by filling the pores with a getter for halogens, such as hydrogen ions. The hydrogen ions adsorbed on the surface of the aluminum oxide react with halogens to form volatile hydrogen halides that can be pumped away in the exhaust system of the semiconductor processing chambers, thereby preventing or reducing reaction of the underlying aluminum oxide with the halogens.

## Claims

### Claim 1

A method of filling in pores in an anodized aluminum part for a vacuum chamber, said part having magnesium oxide deposited on its surface, comprising
a) loading the anodized aluminum part into a vacuum chamber;
b) passing a plasma precursor gas containing fluorine into the chamber while maintaining the chamber at a temperature over 200.degree. C. wherein the pores of said anodized aluminum part are filled with magnesium fluoride.

### Claim 2 (depends on 1)

A method according to claim 1 wherein the temperature of the chamber is maintained at a temperature of from 200.degree. C.-500.degree. C.