# US 5,705,031 A · Process for removing and washing dregs from green liquor in a kraft pulp mill

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- Number: US 5,705,031 A
- Document ID: US5705031A
- Status: Granted
- Kind: A
- Application number: 08/260,327
- Filed: 1994-06-15
- Granted: 1998-01-06
- Earliest claimed: 1994-06-15
- Assignees: Kvaerner Pulping Technologies AB
- Inventors: Peter A. Angevine
- Web page: https://patentgrep.com/patent/US5705031A

## CPC

- D21C 11/0078: {Treatment of green or white liquors with other means or other compounds than gases, e.g. in order to separate solid compounds such as sodium chloride and carbonate from these liquors; Further treatment of these compounds (fractionating of spent liquors D21C11/0042)}
- Y02P 40/40: Production or processing of lime, e.g. limestone regeneration of lime in pulp and sugar mills
- Y10S 210/928: Paper mill waste, e.g. white water, black liquor treated
- D21C: PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- Y02P: CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y10S: TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

## Abstract

In a kraft pulp mill, a process and apparatus for removing and washing dregs from green liquor so that the pH of the dregs is below "hazardous waste" levels. Specifically, green liquor clarifier underflow is filtered using a simple non-precoat cassette filter to form a first dregs cake. The dregs cake is diluted, preferably with water. The diluted dregs cake is then filtered in a precoat dregs filter to produce a dregs cake that is at least 50% solid and has a pH of about 12.0 or less.

## Claims

### Claim 1

In a kraft pulp mill, a process for removing and washing dregs from green liquor comprising the steps of:
clarifying the green liquor in a green liquor clarifier to separate the green liquor into an overflow comprising clarified green liquor and an underflow comprising dregs and green liquor;
filtering the underflow to form a first dregs cake that is at least 50% solid;
diluting the dregs cake to less than 20% solid; and
filtering the diluted dregs cake to form a second dregs cake that is at least 50% solid and has a pH less than 12.5;
wherein the underflow is filtered in a filter that does not use a precoat.

### Claim 2 (depends on 1)

The process of claim 1, wherein the diluted dregs cake is filtered in a precoat filter.

### Claim 3 (depends on 1)

The process of claim 1, wherein the green liquor clarifier underflow contains less than 10% solids.

### Claim 4 (depends on 1)

The process of claim 1, wherein the step of diluting is performed by flushing with water.

### Claim 5

In a kraft pulp mill, a process for removing and washing dregs from green liquor comprising, the steps of:
clarifying the green liquor in a green liquor clarifier to separate the green liquor into an overflow containing clarified green liquor and an underflow containing green liquor and dregs;
filtering the underflow to remove green liquor and form a dregs cake that is at least 50% solid;
flushing the dregs cake with water to dilute the dregs cake; and
dewatering the dregs cake to at least 50% solids and a pH below 12.5;
wherein the green liquor clarifier underflow is filtered by a cassette-type pressure filter.

### Claim 6 (depends on 5)

The process of claim 5, wherein the dregs cake formed by filtering the underflow is diluted to less than 20% solid.

### Claim 7 (depends on 5)

The process of claim 5, wherein the diluted dregs cake is dewatered in a precoat filter.