# US 5,704,227 A · Method of condensing a volatile compound out of a gas stream and an apparatus for this purpose > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 5,704,227 A - Document ID: US5704227A - Status: Granted - Kind: A - Application number: 08/630,366 - Filed: 1996-04-10 - Granted: 1998-01-06 - Earliest claimed: 1995-04-11 - Inventors: Peter Jozef Krabbendam - Web page: https://patentgrep.com/patent/US5704227A ## CPC - B01D 5/0084: {Feeding or collecting the cooling medium (B01D5/0087 takes precedence)} - B01D 5/0036: {Multiple-effect condensation; Fractional condensation} - B01D 5/0051: {Regulation processes; Control systems, e.g. valves} - B01D 5/0096: {Cleaning (cleaning in general B08B)} - B01D 8/00: Cold traps; Cold baffles (pumps for evacuating by condensing or freezing F04B37/08) - F28D 7/106: {consisting of two coaxial conduits or modules of two coaxial conduits} - F28F 27/00: Control arrangements or safety devices specially adapted for heat-exchange or heat-transfer apparatus (control arrangements in general G05) - B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28) - F28D: HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT (fluid heaters having heat generating means and heat transferring means F24H; furnaces F27; details of heat-exchange apparatus of general) - F28F: DETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION (water and air traps, air venting F16) ## Abstract A method and apparatus is provided for the condensation of one or more gasses out of a gas stream. The degree of the condensation of volatile compound out of the gas stream A is controlled by regulating the liquid level of the cooling agent in a heat exchanger (8). Preferably a gas stream A from which the volatile compound has been removed is led to a further heat exchanger (1) and is utilized to pre-cool the gas stream A that is still to be treated. In order to be able to control the degree of condensation of volatile compound out of the gas stream A as accurately as possible, the apparatus is provided with an elongated, vertical heat exchanger (8). ## Claims ### Claim 1 A method of condensing a volatile harmful compound out of an input waste gas stream, said method comprising the steps of: introducing a coolant liquid into a first hollow body of a heat exchanger having a vertical directional component; passing the input waste gas stream through a second hollow body of said heat exchanger, thereby placing the input waste gas stream in thermal communication with said first hollow body; controlling the level of said coolant liquid in said first hollow body of said heat exchanger, thereby controlling the rate of thermal communication between said first hollow body and the input waste gas stream; whereby said level of said coolant liquid within said first hollow body controls the temperature of an output waste gas stream formed by transferring heat from the input waste gas stream. ### Claim 2 (depends on 1) A method according to claim 1 further comprising the step of pre-cooling the input waste gas stream, said step of pre-cooling the input waste gas stream including the steps of: passing the input waste gas stream through a second inlet opening of a further heat exchanger; and passing the output waste gas stream from said heat exchanger through a second inlet opening of said further heat exchanger; whereby the input waste gas stream is pre-cooled by the output waste gas stream from said heat exchanger. ### Claim 3 (depends on 2) A method according to claim 2 wherein the step of pre-cooling the input waste gas stream includes the step of pre-cooling the input waste gas stream to a temperature near but above the dew point of the volatile harmful compound to be removed from the input waste gas stream. ### Claim 4 (depends on 3) A method according to claim 3 further comprising the step of cleaning said second heat exchanger by vaporizing a non-gaseous harmful compound from said second heat exchanger, said cleaning step including the steps of: draining said coolant liquid from said first hollow body of said second heat exchanger; passing the input waste gas stream through a second hollow body of said second heat exchanger, thereby placing the input waste gas stream in thermal communication with the non-gaseous harmful compound; whereby the input waste gas stream vaporizes the non-gaseous harmful compound in said second heat exchanger. ### Claim 5 (depends on 3) A method according to claim 3 further comprising the step of cleaning said second heat exchanger by liquefying frozen harmful compound from said second heat exchanger, said cleaning step including the steps of: draining said coolant liquid from said first hollow body of said second heat exchanger; passing the input waste gas stream through a second hollow body of said second heat exchanger, thereby placing the input waste gas stream in thermal communication with the frozen harmful compound whereby the input waste gas stream liquefies the non-gaseous harmful compound in said second heat exchanger. ### Claim 6 (depends on 1) A method according to claim 1 wherein said step of passing the input waste gas stream through said second hollow body of said heat exchanger comprises the step of leading the input waste gas stream through said second hollow body of said heat exchanger in a downward direction. ### Claim 7 (depends on 1) A method according to claim 1 wherein the coolant liquid is liquefied gas. ### Claim 8 (depends on 1) A method according to claim 1 wherein said coolant liquid is liquid nitrogen. ### Claim 9 An apparatus for creating an output waste gas stream from an input waste gas stream by condensing a volatile harmful compound out of the input waste gas stream, said apparatus comprising: a first heat exchanger having a first inlet opening to admit the input waste gas stream into said first heat exchanger, a first outlet opening for allowing exit of the input waste gas stream from said first heat exchanger, a second inlet opening to admit the output waste gas stream into said first heat exchanger, a second outlet opening for allowing exit of the output waste gas stream from said first heat exchanger, a second heat exchanger having a first hollow body and a second hollow body, said first hollow body arranged in thermal communication with said second hollow body, and said second hollow body having a vertical directional component, a third inlet opening connecting said second hollow body to said first outlet opening of said first heat exchanger, a third outlet opening connecting said second hollow body to said second inlet opening of said first heat exchanger, a drainage outlet connected to said second hollow body to permit drainage of condensate from the input waste gas stream, a fourth inlet opening to allow passage of a liquid coolant into said first hollow body, and a fourth outlet opening to allow passage of gas out of said first hollow body. ### Claim 10 (depends on 9) An apparatus according to claim 9 wherein said first hollow body is located inside said second hollow body so that the input waste gas stream entering said second hollow body through said third inlet opening can be led through said second hollow body in a substantially vertical direction along said first hollow body. ### Claim 11 (depends on 9) An apparatus according to claim 9 wherein said first hollow body is a double-walled hollow body having an inner wall and an outer wall so that said liquid coolant can be introduced through said fourth inlet opening into the space between said inner wall and said outer wall of said first hollow body. ### Claim 12 (depends on 9) An apparatus according to claim 9 wherein said first hollow body is an elongated, vertically placed hollow body. ### Claim 13 (depends on 9) An apparatus according to claim 9 further comprising a third heat exchanger connected in parallel to said second heat exchanger.