# US 5,703,343 A · Process and plant for the manufacture of solid castings from an essentially liquid reactive medium, and oven for heating an essentially liquid medium.

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- Number: US 5,703,343 A
- Document ID: US5703343A
- Status: Granted
- Kind: A
- Application number: 08/545,746
- Filed: 1996-01-30
- Granted: 1997-12-30
- Earliest claimed: 1993-05-05
- Assignees: Ciba Specialty Chemicals Corporation
- Inventors: Mohamad Mallah; Horst Linn; Niklaus Saner; Peter Voirol
- Web page: https://patentgrep.com/patent/US5703343A

## CPC

- H05B 6/802: {for heating fluids (methods of heating fluids in conventional microwave ovens H05B6/687)}
- B29B 13/08: by using wave energy or particle radiation
- B29C 39/006: {Monomers or prepolymers (by reaction injection moulding B29C67/246)}
- B29C 39/24: Feeding the material into the mould
- H05B 6/70: Feed lines
- H05B 6/705: {using microwave tuning}
- H05B 6/707: {using waveguides}
- H05B 6/806: {for laboratory use}
- B29C 2035/0283: {Thermal pretreatment of the plastics material}
- B29C 2035/0855: {using microwave}
- B29K 2105/0002: {monomers or prepolymers}
- H05B: ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- B29B: PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29C: SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING (making preforms B29B11/00; making laminated products by combining previously unconnected layers which become one product whose layers will remain together B32B37/00 - B32B41/00)
- B29K: INDEXING SCHEME ASSOCIATED WITH SUBCLASSES B29B, B29C OR B29D, RELATING TO MOULDING MATERIALS OR TO MATERIALS FOR {MOULDS, } REINFORCEMENTS, FILLERS OR PREFORMED PARTS, e.g. INSERTS

## Abstract

The present invention relates to a process for the manufacture of castings from an essentially liquid reactive medium as casting material which, above its gelation temperature, reacts to form a solid material. The liquid reactive medium is fed from a supply tank, in which the temperature of the casting material lies substantially below its gelation temperature. The liquid reactive medium is fed into a casting mould which has been heated to a temperature that lies above the gelation temperature of the casting material. The casting material is substantially preheated directly before it enters the casting mold to a temperature close to but below the gelation temperature of the casting material.

## Claims

### Claim 1

A process for manufacturing of castings from an essentially liquid reactive medium as casting material which, above its gelation temperature, reacts to form a solid material, in which process the medium is fed from a supply tank (1), in which the temperature of the casting material lies substantially below its gelation temperature, to a casting mould (5) of which the temperature lies above the gelation temperature of the casting material, characterized in that the casting material is substantially preheated directly before it enters the casting mould (5) to a temperature close to but below the gelation temperature of the casting material so that it is still in a state suitable to be fed into the casting mould (5).

### Claim 2 (depends on 1)

A process according to claim 1, wherein there is used as casting material a mixture of hexahydrophthalic acid diglycidyl ester, hexahydrophthalic acid anhydride, benzyldimethylamine and a silanised quartz powder, in a ratio of approximately 100 parts by weight of hexahydrophthalic add diglycidyl ester, approximately 90 parts by weight of hexahydrophthalic acid arthydride; approximately 0.5 parts by weight of benzyldimethylamine; approximately 285 parts by weight silanised quartz powder, and wherein the temperature of the casting material in the supply tank (1) is approximately from 30.degree. C. to 60.degree. C. and wherein during the preheating operation the casting material is heated to a temperature of approximately from 90.degree. C. to 110.degree. C. and the preheated casting material is then fed to the casting mould (5), the temperature of which is approximately from 130.degree. C. to 150.degree. C.

### Claim 3 (depends on 2)

A process according to claim 2 in which the temperature of the casting material in the supply tank is approximately from 40.degree. C. to 50.degree. C.

### Claim 4 (depends on 2)

A process according to claim 2 wherein during the preheating operation the casting material is heated to a temperature of approximately from 95.degree. C. to 100.degree. C.

### Claim 5 (depends on 2)

A process according to claim 2 wherein the preheated casting material is fed to the casting mould at a temperature of approximately from 140.degree. C. to 145.degree. C.
