# US 5,702,499 A · Waste conversion by liquid thermophilic aerobic digestion

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- Number: US 5,702,499 A
- Document ID: US5702499A
- Status: Granted
- Kind: A
- Application number: 08/329,735
- Filed: 1994-10-26
- Granted: 1997-12-30
- Earliest claimed: 1994-01-18
- Assignees: Sim Associates
- Inventors: Hubert J. Timmenga
- Web page: https://patentgrep.com/patent/US5702499A

## CPC

- C05F 17/70: Controlling the treatment in response to process parameters
- A23K 10/12: by fermentation of natural products, e.g. of vegetable material, animal waste material or biomass
- C05F 17/40: Treatment of liquids or slurries
- Y02P 20/145: the feedstock being materials of biological origin
- Y02W 30/40: Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
- C05F: ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- A23K: FODDER
- Y02P: CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02W: CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT

## Abstract

A batch process for the conversion of organic solid waste material containing cellulose and lignin through liquid thermophilic aerobic digestion comprises comminuting the organic solid waste material, adjusting the moisture content of the comminuted material to at least 90% parts by weight of water, mixing the comminuted material with a thermophilic aerobic micro-organism, adjusting the pH of the mixture to 5.5-7.5 and supplying heat and oxygen to the mixture to effect thermophilic aerobic digestion of the mixture. The thermophilic aerobic digestion of the mixture is terminated after the mixture has stabilized as a low nitrogen material but prior to digestion of the cellulose and lignin in the mixture, and the stabilized mixture is separated into solid and liquid fractions. The process includes the monitoring of parameters for determining the termination of digestion.

## Claims

### Claim 1

An aerobic batch process for the conversion of organic solid waste material by liquid thermophilic and solely aerobic digestion, comprising the steps of:
comminuting a batch of the organic solid waste material:
adjusting the moisture content of the comminuted material to at least 90% parts by weight of water;
mixing the comminuted waste material with a thermophilic aerobic micro-organism;
adjusting the pH of the mixture to 5.5-7.5;
supplying heat and oxygen to the mixture to effect thermophilic and solely aerobic digestion of the mixture;
testing the mixture during the aerobic digestion to detect when the mixture has reached a stabilized state in which available organic material and nutrients in the mixture have been consumed by the micro-organisms and in which the micro-organisms have not started to consume lignin or cellulose to any substantial extent;
the testing comprising measuring at least one of the pH level, the phosphate content, the nitrate content, the sulphate content and the carbon-to-nitrogen ratio of the mixture;
terminating the thermophilic and solely aerobic digestion process when the stabilized state is detected; and
subsequently drying the mixture.

### Claim 2 (depends on 1)

A batch process as claimed in claim 1, in which the step of testing comprises detecting an increase in the pH level of the mixture.

### Claim 3 (depends on 1)

A batch process as claimed in claim 1, in which the step of testing comprises detecting a decrease to substantially zero of the phosphate content of the mixture.

### Claim 4 (depends on 1)

A batch process as claimed in claim 1, in which the step of monitoring comprises detecting a peak in the sulphate content.

### Claim 5 (depends on 1)

A batch process as claimed in claim 1, in which the monitoring step comprises detecting termination of a decrease of the carbon-to-nitrogen ratio.

### Claim 6 (depends on 1)

A batch process as claimed in claim 1, which includes adjusting of the carbon-to-nitrogen ratio of the mixture by adding carbon-rich material to the mixture.

### Claim 7 (depends on 1)

A batch process as claimed in claim 1, which includes adjusting of the carbon-to-nitrogen ratio of the mixture by adding nitrogen-rich material to the mixture.

### Claim 8 (depends on 1)

A batch process as claimed in claim 1, which includes screening the stabilized mixture to remove contaminants.

### Claim 9 (depends on 1)

A batch process as claimed in claim 1, in which vapour formed during the liquid thermophilic aerobic digestion and the drying is condensed and discharged without further treatment.

### Claim 10 (depends on 1)

A batch process as claimed in claim 1, in which heat produced by the liquid thermophilic aerobic digestion is employed to heat further waste material prior to the digestion of the further waste material.

### Claim 11 (depends on 1)

A batch process as claimed in claim 1, in which gases given off by the waste material prior to the liquid thermophilic aerobic digestion are collected and injected into the mixture as the mixture undergoes the liquid thermophilic aerobic digestion.