# US 5,700,359 A · Method of polarizing at least one large area sheet of ferroelectric material

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- Number: US 5,700,359 A
- Document ID: US5700359A
- Status: Granted
- Kind: A
- Application number: 08/604,027
- Filed: 1996-02-20
- Granted: 1997-12-23
- Earliest claimed: 1995-02-17
- Assignees: Institut Franco-Allemand de Recherches de Saint-Louis
- Inventors: Fran.cedilla.ois Bauer
- Web page: https://patentgrep.com/patent/US5700359A

## CPC

- H10N 30/098: Forming organic materials
- H10N 30/045: by polarising
- H10N 35/01: Manufacture or treatment
- Y10T 29/42: Piezoelectric device making
- H10N: ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
- Y10T: TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION

## Abstract

A method of polarizing at least one large area sheet of ferroelectric material (1). The method comprises the following successive steps: placing films of ferroelectric material (2, 3) of thickness e.sub.1 against two opposite faces (1a, 1b) of the sheet (1) of thickness e.sub.2, the thickness e.sub.1 being a function of the respective coercive fields of the materials constituting the sheet (1) and the films (2, 3); placing electrodes (4, 5) on either side of and against the films of ferroelectric material (2, 3); compressing the resulting complex; and applying a cyclical voltage between the two electrodes (4, 5).

## Claims

### Claim 1

A method of polarizing at least one sheet of ferroelectric material having an area, the method comprising the following successive steps:
placing a film of ferroelectric material of film thickness e.sub.1 against each of opposite faces of the sheet of sheet thickness e.sub.2, the film thickness e.sub.1 being a function of the sheet thickness e.sub.2 and of a coercive field of each material of the sheet and of the films, the sheet of ferroelectric material and the films of ferroelectric material being made of different substances;
placing an electrode against a side of each film of ferroelectric material remote from said sheet to form an assemembly;
compressing the assembly; and
applying a cyclical electric voltage between the two electrodes to polarize said sheet of ferroelectric material.

### Claim 2 (depends on 1)

A method according to claim 1, wherein said films are made of a ferroelectric material whose coercive field is less than the coercive field of the ferroelectric material of the sheet, and the film thickness e.sub.1 is at least equal to the sheet thickness e.sub.2.

### Claim 3 (depends on 1)

A method according to claim 1, wherein said films are made of a ferroelectric material whose coercive field is greater than the coercive field of the ferroelectric-material of the sheet, and the film thickness e.sub.1 is at most equal to the sheet thickness e.sub.2.

### Claim 4 (depends on 1)

A method according to claim 1, wherein each of the films of ferroelectric material has an area which is at least equal to the area of the sheet of ferroelectric material.

### Claim 5 (depends on 1)

A method according to claim 1, wherein each of the electrodes has an area which is less than the area of the sheet of ferroelectric material.

### Claim 6 (depends on 1)

A method according to claim 1, wherein the films of ferroelectric material are films that are already polarized.

### Claim 7 (depends on 1)

A method according to claim 1, wherein the sheet, the films of ferroelectric material, or both are single or double-stretched.

### Claim 8 (depends on 1)

A method according to claim 1, wherein the ferroelectric material of the films is a copolymer.

### Claim 9 (depends on 1)

A method according to claim 1, wherein the ferroelectric material of the sheet is a polymer.

### Claim 10 (depends on 1)

A method according to claim 1, wherein the ferroelectric material of the sheet is a copolymer.

### Claim 11 (depends on 1)

A method according to claim 1, wherein the ferroelectric material of the sheet is a composite polymer filled with magnetostrictive oxides, or a copolymer coated in a protective polymer.

### Claim 12 (depends on 1)

A method according to claim 1, wherein the sheet of ferroelectric material is not coated in a liquid dielectric insulator.

### Claim 13 (depends on 1)

A method according to claim 1, wherein the assembly is compressed as a function of a desired level of polarization.

### Claim 14 (depends on 1)

A method according to claim 1, wherein the films of ferroelectric material are already polarized, and the electric voltage between the electrodes is applied in a direction indicated by a piezoelectric field created by compression of the assembly.