# US 5,699,679 A · Cryogenic aerosol separator > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 5,699,679 A - Document ID: US5699679A - Status: Granted - Kind: A - Application number: 08/691,702 - Filed: 1996-07-31 - Granted: 1997-12-23 - Earliest claimed: 1996-07-31 - Assignees: International Business Machines Corporation - Inventors: Jin Jwang Wu; William Albert Cavaliere; James Patrick Norum; Stefan Schmitz - Web page: https://patentgrep.com/patent/US5699679A ## CPC - B07B 7/00: Selective separation of solid materials carried by, or dispersed in, gas currents (sieves or filters for separating dispersed particles from gases or vapours B01D) - B07B: SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL (wet separating processes, sorting by processes using fluent material in the same way as liquid B03; combinations of dry separating apparatus with wet separating apparatus B03B; using liquids B03B, B03D; sorting by magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high voltage electric fields B03C; centrifuges or vortex apparatus for carrying out physical processes B04; hand sorting, postal sorting, sorting by switching or other devices actuated in response to detection or measurement of some feature of articles or samples of material B07C) ## Abstract A cryogenic aerosol separator/classifier for separating and selectively removing particles from a stream of aerosol. The aerosol stream is produced by a cryogenic aerosol generator comprising a reservoir containing a cryogenic gas-liquid mixture at a first pressure, a delivery line coupled to the reservoir, and a nozzle. The nozzle has at least one exit opening which allows the cryogenic gas-liquid mixture to expand from the first pressure to a lower pressure and, thus, to produce cryogenic aerosol. A separator is coupled to the nozzle, such that the light particles having high mobility are removed from the stream, thereby producing a stream of cryogenic flow with particles having a controlled size to clean a contaminated surface. The apparatus is enhanced by utilizing a magnetic field and/or specially designed flow fields to fully take advantage of the enhanced mobilities of light particles. ## Claims ### Claim 1 A cryogenic aerosol classifier for inertially separating and classifying particles from a stream of aerosol, comprising: cryogenic aerosol generating means for expanding a cryogenic gas-liquid mixture at a first pressure to a second pressure lower than said first pressure, thereby generating a stream of aerosol having high and low mobility particles; and separator means provided with a diverter coupled to said cryogenic aerosol generating means for removing and diverting particles having high mobility from said stream of aerosol. ### Claim 2 (depends on 1) The cryogenic aerosol classifier according to claim 1, wherein said cryogenic aerosol comprises particles of different sizes. ### Claim 3 (depends on 1) The cryogenic aerosol classifier according to claim 1, wherein said cryogenic aerosol comprises small and large cryogenic particles, said separator means removing said small cryogenic particles from said large cryogenic particles. ### Claim 4 (depends on 3) The cryogenic aerosol classifier according to claim 3, wherein the mass flow rate of the gas stream carrying said large particles is given by the equation .rho.q, with .rho. being the gas density and q, the reduced gas flow rate carrying said large particles. ### Claim 5 (depends on 3) The cryogenic aerosol classifier according to claim 3, wherein said separator means comprises a vacuum for separating said small particles. ### Claim 6 (depends on 3) The cryogenic aerosol classifier according to claim 3, wherein said diverter comprises at least one side passage integral to said nozzle. ### Claim 7 (depends on 3) The cryogenic aerosol classifier according to claim 3, further comprising a plurality of side passages connected at periodic intervals of said separator means to classify said cryogenic aerosol in accordance to the size and the mobility of said particles comprising said aerosol. ### Claim 8 (depends on 1) The cryogenic aerosol classifier according to claim 1, further comprising magnetic means surrounding the periphery of said separator means for increasing the mobility of said particles having high mobility. ### Claim 9 (depends on 8) The cryogenic aerosol classifier according to claim 8, wherein said magnetic means deflect particles having a lower mass/charge ratio to a greater extent than particles having a higher mass/charge ratio. ### Claim 10 (depends on 1) The cryogenic aerosol classifier according to claim 1, wherein said cryogenic gas-liquid mixture is selected from the group consisting of carbon dioxide, argon, nitrogen and mixtures thereof. ### Claim 11 (depends on 1) The cryogenic aerosol classifier according to claim 1, further comprising a reservoir wherein said gas-liquid mixture is maintained at cryogenic temperature. ### Claim 12 (depends on 1) The cryogenic aerosol classifier according to claim 1, further comprising a cross-stream gas flow into an outlet positioned downstream from said nozzle to divert said particles of high mobility from said stream of aerosol. ### Claim 13 (depends on 12) The cryogenic aerosol classifier according to claim 12, wherein said outlet is positioned opposite to an inlet carrying said cross-stream gas. ### Claim 14 A cryogenic aerosol classifier for inertially separating and classifying particles from a stream of aerosol, comprising: a cryogenic aerosol generator comprising a reservoir containing a cryogenic gas-liquid mixture at a first pressure, a delivery line coupled to said reservoir, and a nozzle connected to said delivery line for expanding said mixture from said first pressure to a second pressure lower than said first pressure for producing a cryogenic aerosol having high and low mobility particles; and separator means provided with a diverter, said separator means being coupled to said nozzle, wherein particles having high mobility are removed and diverted from said stream. ### Claim 15 (depends on 14) The cryogenic aerosol classifier according to claim 14, wherein said diverter comprises at least one side passage integral to said nozzle. ### Claim 16 (depends on 14) The cryogenic aerosol classifier according to claim 14, wherein said separator means comprises a vacuum for separating said high mobility particles. ### Claim 17 (depends on 14) The cryogenic aerosol classifier according to claim 14, further comprising a plurality of side passages connected at periodic intervals of said nozzle to classify said cryogenic particles in accordance to their size and their mobility. ### Claim 18 (depends on 14) The cryogenic aerosol classifier according to claim 14, further comprising a heat exchanger coupled to said reservoir and to said nozzle for receiving and cooling said gas-liquid mixture or gas to a cryogenic temperature. ### Claim 19 A method for separating and classifying cryogenic aerosol particles having different mobility, comprising the steps of: generating an aerosol having high and low mobility particles by moving a cryogenic gas-liquid mixture from an area at a first pressure into an area at a second pressure which is lower than said first pressure; and providing a separator having a diverter to separate from said aerosol particles having high mobility from particles having a low mobility. ### Claim 20 (depends on 19) The method according to claim 19, wherein said separator means comprises a vacuum for separating said high mobility particles. ### Claim 21 (depends on 19) The method according to claim 19, wherein said separator comprises at least one side passage. ### Claim 22 (depends on 19) The method according to claim 19, wherein said separator further comprising a plurality of side passages connected at periodic intervals to classify said aerosol in accordance to the size and the mobility of said particles comprising said aerosol. ### Claim 23 (depends on 19) The method according to claim 19, further comprising magnetic means surrounding the periphery of said separator for increasing the mobility of said particles having high mobility. ### Claim 24 (depends on 23) The method according to claim 23, wherein said magnetic means deflect particles having a lower mass/charge ratio to a greater extent than particles having a higher mass/charge ratio. ### Claim 25 (depends on 19) The method according to claim 19, wherein said cryogenic gas-liquid mixture is selected from the group consisting of carbon dioxide, argon, nitrogen and mixtures thereof. ### Claim 26 (depends on 19) The cryogenic aerosol classifier according to claim 19, further comprising a reservoir wherein said gas-liquid mixture is maintained at cryogenic temperature. ### Claim 27 A method for separating and classifying cryogenic aerosol, said aerosol having particles with different mobility, said method comprising the steps of: generating aerosol by moving a cryogenic gas-liquid mixture from a reservoir to a delivery line, wherein said delivery line is at a first pressure; moving said mixture from said delivery line through a nozzle into an expansion area such that said mixture is at a second pressure which is lower than said first pressure, thereby creating aerosol particles having particles with different mobility; providing a separator having a diverter coupled to said expansion area for separating the aerosol particles having high mobility from particles having a low mobility; and diverting said particles having high mobility from said expansion area into an outlet, wherein said outlet is at a third pressure which is lower than said second pressure. ### Claim 28 (depends on 27) The method according to claim 27, wherein said third pressure is vacuum. ### Claim 29 (depends on 27) The method according to claim 27, further comprising a cross-stream gas flow into an outlet positioned downstream from said nozzle to divert said particles of high mobility from said stream of aerosol.