Process for producing quarternary ammonium compounds
AssigneesWitco Corporation, Rheox, Inc.
InventorsCharles Cody, N. Ben Martin
Life of this patent
Estimating the term…
Loading patent…
AssigneesWitco Corporation, Rheox, Inc.
InventorsCharles Cody, N. Ben Martin
Estimating the term…
Process for the preparation of quaternary ammonium compounds, by preparing a mixture of a tertiary amine and a liquid reaction vehicle and adding an alkyl halide to the mixture to produce a quaternary ammonium halide, the liquid reaction medium being a liquid, low volatility, substantially non-toxic diluent having a vapor pressure not greater than about 1 mm. Hg at a temperature of 25.degree. C. and preferably being a fatty acid or a fatty acid mono-, di-, or triglyceride, a mineral oil, or 2-ethylhexanol wherein the alkyl groups comprising the fatty acids or the triglycerides have from about 10 to about 24 carbon atoms, the quaternary ammonium compounds being particularly suited for uses such as deinking of paper in conjunction with appropriate clays, surfactants, flotation agents, anti-static agents and biocides.
In a process for the preparation of quaternary ammonium halide compound which comprises preparing a mixture consisting essentially of an amine, a diluent, and an alkyl halide alkylating agent to produce a quaternary ammonium halide compound, and thereafter recovering said quaternary ammonium halide compound, the improvement comprising the diluent being selected from the group consisting of fatty acid triglycerides and 2-ethylhexanol.
In a process for the preparation of a quaternary ammonium composition which comprises preparing a mixture consisting essentially of an amine, a diluent, and an alkyl halide alkylating agent to produce said quaternary ammonium composition, the improvement comprising the diluent being selected from the group consisting of fatty acid triglycerides and 2-ethylhexanol.
The process of 19, wherein the amine is a tertiary amine having the formula ##STR3## wherein R.sup.1 is lower alkyl;
Dependencies are inferred from the claim text.