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US 5,691,408 AGranted
Process for manufacturing water based adhesive
AssigneeAkron Paint & Varnish
InventorRobert J. Murray
Life of this patent
Estimating the term…
Abstract
A process for manufacturing a water based adhesive which is substantially free of organic solvents and is useful as an adhesive for bonding natural rubber compounds, synthetic rubber compounds and a combination of natural and synthetic rubber compounds, especially during the formation of a tire.
Claims22
A process for manufacturing a water based adhesive having essentially no organic solvents contained therein, said process comprising the steps of:
- (1) supplying an elastomer emulsion, said elastomer emulsion having a measure pH within the range of 9.0 to 12.0;
- (2) preparing a water solution comprising water and a pH adjuster, said pH adjuster being added to said water in an effective amount to adjust the pH of said water solution to within about .+-.10% of the measured pH of said elastomer emulsion;
- (3) preparing a carbon black dispersion comprising carbon black, water, and surfactants, said carbon black dispersion having a pH within about .+-.10% of the measured pH of said elastomer emulsion;
- (4) mixing said elastomer emulsion of Step (1) with said water solution of Step (2), and the carbon black dispersion of Step (3) to form said water based adhesive;
- and
- wherein the water based adhesive of Step (4) comprises:
- from about 25.0 to about 50.0%, by weight, of an elastomer selected from the group consisting of natural rubber, synthetic rubber, butadiene rubber, polybutadiene rubber and mixtures thereof;
- from about 40.0 to about 60.0%, by weight, water;
- and
- from about 0.5 to about 10.0%, by weight, carbon black.
7 more elements
A process for manufacturing a water based adhesive having essentially no organic solvents contained therein, said process comprising the steps of:
- (1) supplying an elastomer emulsion, said elastomer emulsion having a measure pH within the range of 9.0 to 12.0;
- (2) preparing a water solution comprising water and a pH adjuster, said pH adjuster being added to said water in an effective mount to adjust the pH of said water solution to within about .+-.10% of the measured pH of said elastomer emulsion;
- (3) preparing a carbon black dispersion comprising carbon black, water, surfactants, and a pH adjuster, said pH adjuster being added to said dispersion in an effective mount so as to yield a pH of said dispersion within about .+-.10% of the measured pH of said elastomer emulsion;
- (4) mixing said elastomer emulsion of Step (1) with said water solution of Step (2) to create an elastomer emulsion/water solution mixture;
- (5) mixing said carbon black dispersion of Step (3) with the elastomer emulsion/water solution mixture of Step (4) to form said water based adhesive;
- and
- wherein the water based adhesive of Step (5) comprises:
- from about 25.0 to about 50.0%, by weight, of an elastomer selected from the group consisting of natural rubber, synthetic rubber, butadiene rubber, polybutadiene rubber and mixtures thereof,
- from about 40.0 to about 60.0%, by weight, water;
- and
- from about 0.5 to about 10.0%, by weight, carbon black, said carbon black being selected from the group consisting of N-300 and N-200 series and mixtures thereof.
8 more elements
Dependencies are inferred from the claim text.