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US 5,672,776 AGranted
Method for purifying 1,1,1-tris(4-hydroxyphenyl)-alkanes
AssigneeGeneral Electric Company
InventorsPatrick Joseph McCloskey, Julia Lam Lee
Life of this patent
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Abstract
Tris(4-hydroxyphenyl)alkanes such as 1,1,1 -tris(4-hydroxyphenyl)ethane are purified by formation of an adduct with a molar excess of a C.sub.1-4 primary alkyl tertiary amine, preferably triethylamine. Adduct formation is preferably effected in a polar organic solvent such as methanol. The pure tris(4-hydroxyphenyl)alkane may be recovered from the adduct by thermal or aqueous acid-promoted cracking.
Claims15
A method for further purifying a tris(4-hydroxyphenyl)alkane of at least about 90% by weight purity which comprises:
- forming an adduct by contacting said tris(4-hydroxyphenyl)alkane with a molar excess of a C.sub.1-4 primary alkyl tertiary amine, and
- recovering purified tris(4-hydroxyphenyl)alkane from said adduct by thermal or aqueous acid-promoted cracking.
Dependencies are inferred from the claim text.