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US 5,645,782 AGranted
Process for making poly(trimethylene terephthalate) bulked continuous filaments
AssigneeE. I. Du Pont de Nemours and Company
InventorsJames Milton Howell, Wae-Hai Tung, Frank Werny
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Abstract
Polyester carpets of poly(trimethylene terephthalate) are disclosed which have excellent stain-resistance, texture retention and resistance to crushing. The bulked continuous filament yarn used to make the carpets and the process for making the yarns are also disclosed.
Claims10
A process for the production of poly(trimethylene terephthalate) bulked continuous filaments comprising the steps of:
- a) extruding molten poly(trimethylene terephthalate) polymer at a temperature from 245.degree. C. to 285.degree. C. through a spinneret to form filaments, said poly(trimethylene terephthalate) polymer having an intrinsic viscosity in the range of 0.6 to 1.3 and a water content of less than 100 ppm by weight;
- b) cooling the filaments in a quench chimney by means of air flowing perpendicularly to the filaments at a velocity in the range of 0.2 to 0.8 m/sec.;
- c) coating the filaments with a spin finish;
- d) heating the filaments to a temperature greater than the glass transition temperature of the filaments, but less than 200.degree. C. prior to drawing the filaments;
- e) drawing the filaments between a set of feed rolls and a set of draw rolls to a draw ratio high enough that the break elongation of the drawn filaments is between 10 to 90%, the temperature of the draw rolls being from 120.degree. to 200.degree. C.;
- f) feeding the drawn filaments from the draw rolls at a speed of at least 800 m/min. to a hot-fluid jet bulking unit in which the filaments are blown and deformed in three dimensions with hot bulking fluid having a temperature at least as high as that of the draw rolls to form bulked continuous filaments having random 3-dimensional curvilinear crimp;
- g) cooling the bulked continuous filaments to a temperature less than the glass transition temperature of the filaments;
- h) winding up the filaments at a speed at least 10% lower than that of the draw rolls.
5 more elements
Dependencies are inferred from the claim text.