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US 5,538,594 AGranted
Method for producing a blade coated paper from recycled, high lignin content, waste paper
AssigneeWestvaco Corporation
InventorsMark A. Hank, Leo T. Mulcahy, Ralph S. Peterson, Robert C. Streisel
Life of this patent
Estimating the term…
Abstract
A method is disclosed for producing, in a continuous throughput, high quality paper from recycled waste paper utilizing high consistency, low shear pulping, followed by a series of cleaning steps to produce a wet, friable pulp which is digested and optionally bleached. The resulting pulp can be run on a paper machine alone or blended with virgin pulp to produce a paper containing at least 10% by weight recycled paper with less than 20 ppm per unit area solid non-fibrous contaminants larger than 0.3 mm.sup.2, and which may be blade coated on a high speed paper machine.
Claims21
A method for preparing a blade-coated paper having less than 20 ppm per unit area solid, non-fibrous contaminants of a size greater than 0.05 mm.sup.2, and including a furnish having at least 10% by weight recycled paper substantially comprised of corrugated containers to be recycled, consisting essentially of the steps of:
- a) combining a quantity of paper substantially comprised of corrugated containers to be recycled, containing lignin, cellulosic fibers and solid non-fibrous contaminants, with an aqueous liquid to form a slurry containing about 9-15% by weight solids and agitating said slurry in a low shear mixer at a temperature of less than 65.5.degree. C. for a time sufficient to separate said lignin and cellulosic fibers from said solid contaminants without significantly degrading said solid contaminants, and then sequentially;
- b) removing from said slurry gross contaminants of a size in a range greater than about 5 mm.sup.2 by passing said slurry through holes of a predetermined diameter;
- c) removing from said slurry contaminants having a specific gravity in a range greater than 1;
- d) removing from said slurry intermediate contaminants having a size in a range greater than about 2 to 3 mm.sup.2 by passing said slurry through holes of a predetermined size;
- e) removing sand from said slurry;
- f) removing from said slurry fine contaminants of a size in a range at least about 0.15 mm.sup.2, by passing said slurry through elongated slots of a predetermined width;
- g) removing from said slurry by centrifugal means contaminants having a specific gravity less than 1;
- h) dewatering said slurry to form a wet, friable pulp having a moisture content of about 30-60%;
- i) digesting said pulp in a cooking liquor for a time and at a temperature sufficient to hydrolyze a substantial portion of said lignin remaining in intimate association with said cellulosic fibers wherein said digesting takes place at a target temperature in a range of 121.degree.-150.degree. C.;
- j) separating said digested pulp from spent cooking liquor;
- k) preparing paper from said separated pulp such that said paper includes at least 10% by weight of said recycled paper substantially comprised of corrugated containers to be recycled;
- and
- l) coating said paper with a clay-containing coating using a blade to regulate coating weight.
10 more elements
A method for preparing a blade-coated paper having less than 20 ppm per unit area solid, non-fibrous contaminants of a size greater than 0.05 mm.sup.2, and including a furnish having at least 10% by weight recycled paper substantially comprised of corrugated containers to be recycled, comprising the steps of:
- a) combining a quantity of paper substantially comprised of corrugated containers to be recycled, containing lignin, cellulosic fibers and solid non-fibrous contaminants, with an aqueous liquid to form a slurry containing about 9-15% by weight solids and agitating said slurry in a low shear mixer at a temperature of less than 65.5.degree. C. for a time sufficient to separate said lignin and cellulosic fibers from said solid contaminants without significantly degrading said solid contaminants, and then sequentially;
- b) removing from said slurry gross contaminants of a size in a range greater than about 5 mm.sup.2 by passing said slurry through holes of a predetermined diameter;
- c) removing from said slurry contaminants having a specific gravity in a range greater than 1;
- d) removing from said slurry intermediate contaminants having a size in a range greater than about 2 to 3 mm.sup.2 by passing said slurry through holes of a predetermined size;
- e) removing sand from said slurry;
- f) removing from said slurry fine contaminants of a size in a range at least about 0.15 mm.sup.2, by passing said slurry through elongated slots of a predetermined width;
- g) removing from said slurry by centrifugal means contaminants having a specific gravity less than 1;
- h) dewatering said slurry to form a wet, friable pulp having a moisture content of about 30-60%;
- i) digesting said pulp in a cooking liquor for a time and at a temperature sufficient to hydrolyze a substantial portion of said lignin remaining in intimate association with said cellulosic fibers wherein said digesting takes place at a target temperature in a range of 121.degree.-150.degree. C.;
- j) separating said digested pulp from spent cooking liquor;
- k) preparing paper from said separated pulp such that said paper includes at least 10% by weight of said recycled paper substantially comprised of corrugated containers to be recycled;
- and
- l) coating said paper with a clay-containing coating using a blade to regulate coating weight.
10 more elements
A method for preparing a blade-coated paper having less than 20 ppm per unit area solid, non-fibrous contaminants of a size greater than 0.05 mm.sup.2, and including a furnish having at least 10% by weight recycled paper substantially comprised of corrugated containers to be recycled, comprising the steps of:
- a) combining a quantity of paper substantially comprised of corrugated containers to be recycled, containing lignin, cellulosic fibers and solid non-fibrous contaminants, and at least 50% by weight of said paper to be recycled originating from said recycled containers, with an aqueous liquid to form a slurry containing about 9-15% by weight solids and agitating said slurry in a low shear mixer at a temperature of less than 65.5.degree. C. for a time sufficient to separate said lignin and cellulosic fibers from said solid contaminants without significantly degrading said solid contaminants, and then sequentially;
- b) removing from said slurry gross contaminants of a size in a range greater than about 5 mm.sup.2 by passing said slurry through holes of a predetermined diameter;
- c) removing from said slurry contaminants having a specific gravity in a range greater than 1;
- d) removing from said slurry intermediate contaminants having a size in a range greater than about 2 to 3 mm.sup.2 by passing said slurry through holes of a predetermined size;
- e) removing sand from said slurry;
- f) removing from said slurry fine contaminants of a size in a range at least about 0.15 mm.sup.2, by passing said slurry through elongated slots of a predetermined width;
- g) removing from said slurry by centrifugal means contaminants having a specific gravity less than 1;
- h) dewatering said slurry to form a wet, friable pulp having a moisture content of about 30-60%;
- i) digesting said pulp in a cooking liquor for a time and at a temperature sufficient to hydrolyze a substantial portion of said lignin remaining in intimate association with said cellulosic fibers wherein said digesting takes place at a target temperature in a range of 121.degree.-150.degree. C.;
- j) separating said digested pulp from spent cooking liquor;
- k) preparing paper from said separated pulp such that said paper includes at least 10% by weight of said recycled paper substantially comprised of corrugated containers to be recycled;
- and
- l) coating said paper with a clay-containing coating using a blade to regulate coating weight.
10 more elements
A method for preparing a blade-coated paper having less than 20 ppm per unit area solid, non-fibrous contaminants of a size greater than 0.05 mm.sup.2, and including a furnish having at least 10% by weight recycled paper substantially comprised of corrugated containers to be recycled, consisting essentially of the steps of:
- a) combining a quantity of paper substantially comprised of corrugated containers to be recycled, containing lignin, cellulosic fibers and solid non-fibrous contaminants, and at least 50% by weight of said paper to be recycled originating from said recycled containers, with an aqueous liquid to form a slurry containing about 9-15% by weight solids and agitating said slurry in a low shear mixer at a temperature of less than 65.5.degree. C. for a time sufficient to separate said lignin and cellulosic fibers from said solid contaminants without significantly degrading said solid contaminants, and then sequentially;
- b) removing from said slurry gross contaminants of a size in a range greater than about 5 mm.sup.2 by passing said slurry through holes of a predetermined diameter;
- c) removing from said slurry contaminants having a specific gravity in a range greater than 1;
- d) removing from said slurry intermediate contaminants having a size in a range greater than about 2 to 3 mm.sup.2 by passing said slurry through holes of a predetermined size;
- e) removing sand from said slurry;
- f) removing from said slurry fine contaminants of a size in a range at least about 0.15 mm.sup.2, by passing said slurry through elongated slots of a predetermined width;
- g) removing from said slurry by centrifugal means contaminants having a specific gravity less than 1;
- h) dewatering said slurry to form a wet, friable pulp having a moisture content of about 30-60%;
- i) digesting said pulp in a cooking liquor for a time and at a temperature sufficient to hydrolyze a substantial portion of said lignin remaining in intimate association with said cellulosic fibers wherein said digesting takes place at a target temperature in a range of 121.degree.-150.degree. C.;
- j) separating said digested pulp from spent cooking liquor;
- k) preparing paper from said separated pulp such that said paper includes at least 10% by weight of said recycled paper substantially comprised of corrugated containers to be recycled;
- and
- l) coating said paper with a clay-containing coating using a blade to regulate coating weight.
10 more elements
Dependencies are inferred from the claim text.