Crystalline lactitol monohydrate and a process for the preparation thereof, use thereof, and sweetening agent
AssigneeSuomen Xyrofin Oy
InventorsHeikki O. Heikkila, Juha V. Nurmi
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AssigneeSuomen Xyrofin Oy
InventorsHeikki O. Heikkila, Juha V. Nurmi
Estimating the term…
A crystalline lactitol monohydrate having lattice cell constants a =7.815.+-.0.008 .ANG., b=12.682.+-.0.008 .ANG., and c=15.927.+-.0.008 .ANG., and a melting range between 90.degree. and 105.degree. C., and a water content between 4.85 and 5.15%, as well as a process of preparing said crystalline lactitol monohydrate by evaporating the aqueous solution of lactitol to a concentration between 75 and 88% by weight, cooling the resultant mixture at a temperature ranging between 30 and 75.degree. C., subsequently separating the lactitol monohydrate crystals from the mother liquor, and subsequently drying with air having a temperature between 120.degree. C., and a relative humidity between 0 and 40%, for a time period less than 24 hours. The invention also relates to the use of said crystalline lactitol monohydrate as a bulk sweetener for the total or partial replacement of sucrose, in dietetic products, confectionery, bakery products, cereals, desserts, jams, beverages, chocolate, chewing gum and ice-cream, and in pharmaceuticals and cosmetic products, such as tooth paste, as well as a special sweetening agent resembling sucrose, mainly composed of said crystalline lactitol monohydrate.
A substantially pure crystalline lactitol monohydrate having lattice cell constants a=7.815.+-.0.008 .ANG., b=12.682.+-.0.008 .ANG., and c=15.927.+-.0.008 .ANG., and a melting range between 90.degree. and 105.degree. C.
A sweetening agent comprising:
A process of preparing a composition for ingestion by a person comprising adding to an ingredient admixture an amount of crystalline lactitol monohydrate having lattice cell constants a=7.815.+-.0.008 .ANG., b=12.682.+-.0.008 .ANG., and c=15.927.+-.0.008 .ANG., and a melting range between about 90.degree. and 105.degree. C.
A lactitol monohydrate substantially free of lactitol in other hydration states having a melting point between about 94.degree. and 98.degree. C., a solubility in 25.degree. C. water of between about 59 and 60%, and a water content between about 4.85 and 5.15%.
Dependencies are inferred from the claim text.