Toner aggregation processes
AssigneeXerox Corporation
InventorsRaj D. Patel, Michael A. Hopper, Paul J. Gerroir, Grazyna E. Kmiecik-Lawrynowicz
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AssigneeXerox Corporation
InventorsRaj D. Patel, Michael A. Hopper, Paul J. Gerroir, Grazyna E. Kmiecik-Lawrynowicz
Estimating the term…
A process for the preparation of toner compositions consisting essentially of (i) preparing a pigment dispersion, which dispersion is comprised of a pigment, an ionic surfactant, and optionally a charge control agent; (ii) shearing said pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant, and a nonionic surfactant; (iii) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution; (iv) subsequently adding further anionic or nonionic surfactant solution to minimize further growth in the coalescence (v); and (v) heating said bound aggregates above about the Tg of the resin and wherein said heating is from a temperature of about 103.degree. to about 120.degree. C., and wherein said toner compositions are spherical in shape.
A process for the preparation of toner compositions consisting essentially of
A process in accordance with claim I wherein the dispersion of (i) is accomplished by an ultrasonic probe at from about 300 watts to about 900 watts of energy, at from about 5 to about 50 megahertz of amplitude, at a temperature of from about 25.degree. C. to about 55.degree. C., and for a duration of from about 1 minute to about 120 minutes.
A process consisting essentially of
Dependencies are inferred from the claim text.