Process for preparing cellulose ethers with cyclic ethers as suspending agents
AssigneeHoechst Aktiengesellschaft
InventorDiethart Reichel
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Abstract
Process for preparing cellulose ethers with cyclic ethers as suspending agents. The present invention relates to a process for preparing cellulose ethers from cellulose and alkylating agents, in the presence of water and bases and at least one water-miscible cyclic ether as the suspending agent, comprising the stages: a) alkalisation, b) subsequent alkylation, wherein the water-miscible cyclic ether is employed already in stage a) or, where appropriate, not until stage b).
Claims18
A process for preparing cellulose ethers from cellulose and alkylating agents, in the presence of a base and water and a water miscible cyclic ether as a suspending agent consisting essentially of dioxane and/or THF comprising the stages:
- a) alkalization,
- b) subsequent alkylation, and optionally stage
- c) hydroxyalkylation which would be performed between stages a) and b);
- wherein the water-miscible cyclic ether is admixed in
- 1) stage a) or,
- 2) if optional stage c) is performed then in stage a) or stage c) , and wherein after stage a) and before stage b) a part of the water-miscible cyclic ether together with a part of the .water are removed by distillation.
The process as claimed in claim 4, wherein up to 70% by weight of the suspending agent/water mixture admixed is removed.
Dependencies are inferred from the claim text.