Method for producing ceramics reinforced with three-dimensional fibers
AssigneesAgency of Industrial Science and Technology, Ministry of International Trade & Industry
InventorsKikuo Nakano, Akira Kamiya
Life of this patent
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Abstract
A method for producing ceramics reinforced with three-dimensional fibers, which entails: a) setting a filter plate in contact with one surface of a three-dimensional fiber preform and a porous metallic plate in contact with said filter plate; b) setting a slurry in contact with a surface of the preform opposite to the one surface; c) exerting pressure on the slurry and, at the same time, subjecting the preform to vacuum aspiration through the filter plate, thereby obtaining a composite having an impregnated preform, the impregnation being effected in a single step; d) heating the composite; and e) firing the resultant composite.
Claims13
A method for the production of ceramics reinforced with three-dimensional fibers, which comprises:
- a) setting a filter plate having pores of not more than about 0.3 .mu.m in diameter in contact with one surface of a three-dimensional fiber preform and a porous metallic plate in contact with said filter plate;
- b) setting a slurry in contact with a surface of said preform opposite to said one surface, said slurry having a concentration within a range of about 100 to 200 g/l and consisting of about 70 to 90% by weight of a fine ceramic powder having a particle diameter in a range of about 0.01 to 3 .mu.m, and about 30 to 10% by weight of an organic silicon resin which is a ceramic precursor, in a solvent;
- c) exerting a pressure of not less than about 400 kgf/cm.sup.2 on said slurry at a pressing speed in a range of about 0.05 to 5 mm/min, at the same time, subjecting said preform to vacuum aspiration through said filter plate, thereby obtaining a composite having said preform impregnated with said fine ceramic powder and said organic silicon resin, said impregnation of said preform being effected in a single step;
- d) heating said composite at a temperature in a range of about 600.degree. to 1,000.degree. C. to thermally decompose said organic silicon resin;
- and
- e) firing the resultant composite at a temperature in a range of about 1,500.degree. to 2,000.degree. C.
Dependencies are inferred from the claim text.