Process for the delignification of cellulose fiber raw materials using alcohol and alkali
OwnerKarl-Heinz Brodersen, Gerhard Dahlmann +1inventors
InventorsKarl-Heinz Brodersen, Gerhard Dahlmann, Heinrich Leopold
Life of this patent
Estimating the term…
Abstract
A process for the delignification of cellulose fiber plant raw material for the production of pulp using separate impregnating and delignifying stages, each using alcohol and alkali. The process may be carried out in batch or in a continuous process. Less alcohol is used in the delignification stage than in the delignification stage. The pulp produced has very good properties because different amounts of alcohol are being used in the impregnation stage and in the delignification stage.
Claims32
A process for the delignification of fibrous material comprising:
- heating a mixture of alcohol and water,
- contacting the fibrous material with impregnation liquor at a temperature in the range of 100.degree.-160.degree. C. in an impregnation stage comprising the addition of said heated mixture of alcohol and water,
- impregnating the fibrous material in the impregnation stage until a phase equilibrium is attained between the impregnation liquor and the liquid contained in the fibrous material,
- heating an aqueous mixture of alkali and alcohol,
- contacting the fibrous material with delignifying liquor in a single delignification stage comprising the addition of said heated aqueous mixture of alkali and alcohol,
- wherein the concentration of alcohol in the delignification stage is lower than the concentration of alcohol in the impregnation stage, and
- the pH in the delignification stage is in the range pH 9-12;
- decreasing uniformly the concentration of alcohol contained in the fibrous material during the delignification stage, and
- steadily increasing the concentration of the alkali in the fibrous material during the initial delignification stage, and then decreasing the concentration of alkali until a phase equilibrium is again reached between the liquid in the fibrous material and the delignification liquor.
A process according to claim 31 in which the liquor-to-wood ratio in the delignification stage is 4.5:1.
Dependencies are inferred from the claim text.