# US 5,417,107 A · Method and capacitance probe arrangement

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- Number: US 5,417,107 A
- Document ID: US5417107A
- Status: Granted
- Kind: A
- Application number: 08/124,957
- Filed: 1993-09-21
- Granted: 1995-05-23
- Earliest claimed: 1993-09-21
- Assignees: Paul-Munroe Engineering
- Inventors: Michael P. Biencourt; John A. DeVries
- Web page: https://patentgrep.com/patent/US5417107A

## CPC

- G01N 27/223: {for determining moisture content, e.g. humidity (rain detectors on vehicle windows B60S1/0825)}
- G01N 33/2823: {Raw oil, drilling fluid or polyphasic mixtures}
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

An improved method and capacitance probe arrangement for determining the fluid phase fractions of fluids having differing permitivity such as those of gas, oil, and water and oil-water emulsion in a fluid stream flowing from an oil well which includes trapping the primarily liquid in a vertically disposed chamber. The liquid is held therein to permit separation of the phase fractions to the extent possible within a reasonable time. A number of measurements are taken of the capacitance at a plurality of discrete vertically spaced locations within the chamber. These capacitance measurements relate directly to the varying permittivity of the phase fractions of the various liquids contained therein which may be gas, oil, and water and a oil-water emulsion. The measurements are processed by a data processor to provide precise information on such phase fractions and emulsion interfaces. A number of embodiments of the novel probe are disclosed for determining capacitance at spaced locations within the chamber. The present method overcomes many of the problems that have plagued prior systems including temperature dependance, fouling of the system by oil build up, lengthy delays of emulsion settling, calibration problems, and changing physical properties of the oil and water in the well stream.

## Claims

### Claim 1

A method for calculating the volumetric phase fractions of a fluid having phase fractions that have different permittivities which comprises:
introducing a sample of such a fluid in a chamber;
measuring the capacitance of the sample at a plurality of points along the vertical height of the chamber;
determining a plurality of other measurements of the contained fluid, said other measurements comprising absolute temperature, absolute pressure and differential pressure generated by known liquid column height, and
employing such capacitance and other measurements to calculate the volummetric fractions of the contained fluid.

### Claim 2 (depends on 1)

The method of claim 1 wherein the measurement of the capacitance of the contained fluid includes disposing an electrically non-conductive tube vertically in the chamber containing the fluid;
introducing an electrically conductive liquid upwardly into the tube, and
measuring the capacitance as the conductive fluid rises in the tube.

### Claim 3 (depends on 2)

The method of claim 2 wherein the introduction step includes introducing brine into the tube.

### Claim 4 (depends on 1)

An arrangement for carrying out the method of claim 1 which includes:
a tank which contains a liquid having volumetric phase fractions that have different permittivities;
a vented hollow electrically non-conductive tube which extends vertically through the tank so as to be in contact with the contained liquid;
a source of an electrically conductive liquid coupled to the bottom of the tube;
a pump means connected to the source of electrically conductive liquid and adapted to pump such liquid upwardly in the tube in a predetermined controlled manner;
other measurements means coupled to the tank for determining said plurality of other measurement values related to the contained liquid, and
calculating means coupled to the capacitance measurement means and to the other measurement means for calculating the volummetric phase fractions of the liquids comprising the contained liquid.

### Claim 5 (depends on 4)

The arrangement of claim 4 wherein the liquid contained in the tank is oil having phase fractions of oil, oil-water emulsion, and water with gas interposed over the liquid.

### Claim 6 (depends on 5)

The arrangement of claim 5 wherein the tank that is provided with a controllable valve interposed at a lower portion and which may be opened in response to the calculating means to permit water to flow from the tank.

### Claim 7 (depends on 1)

The arrangement of claim 1 wherein the sample is held in the chamber for a predetermined time.

### Claim 8

A method for calculating the volumetric phase fractions of a fluid having phase fractions that have different permittivities which comprises:
introducing a sample of such a fluid in a chamber;
measuring the capacitance of the sample at a plurality of points along the vertical height of the chamber by disposing an electrically non-conductive tube vertically in the chamber containing the fluid,
introducing an electrically conductive liquid upwardly into the tube and
measuring the capacitance as the conductive fluid rises in the tube;
determining a plurality of other measurements of the contained fluid said other measurements comprising absolute temperature, absolute pressure and differential pressure generated by known liquid column height, and
employing such capacitance and other measurements to calculate the volumetric fractions of the contained fluid.

### Claim 9 (depends on 8)

The method of claim 8 wherein the introduction step includes introducing brine into the tube.

### Claim 10 (depends on 8)

An arrangement for carrying out the method of claim 8 which includes:
a tank which contains a liquid having volumetric phase fractions that have different permittivities;
a vented hollow electrically non-conductive tube which extends vertically through the tank so as to be in contact with the contained liquid;
a source of an electrically conductive liquid coupled to the bottom of the tube;
a pump means connected to the source of electrically conductive liquid and adapted to pump such liquid upwardly in the tube in a predetermined controlled manner;
other measurements means coupled to the tank for determining said plurality of other measurement values related to the contained liquid, and
calculating means coupled to the capacitance measurement means and to the other measurement means for calculating the volumetric phase fractions of the liquids comprising the contained liquid.

### Claim 11 (depends on 10)

The arrangement of claim 10 wherein the liquid contained in the tank is oil having phase fractions of oil, oil-water emulsion, and water with gas interposed over the liquid.

### Claim 12 (depends on 11)

The arrangement of claim 11 wherein the tank that is provided with a controllable valve interposed at a lower portion and which may be opened in response to the calculating means to permit water to flow from the tank.