# US 5,351,120 A · Spectroscopic cell design

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- Number: US 5,351,120 A
- Document ID: US5351120A
- Status: Granted
- Kind: A
- Application number: 08/090,883
- Filed: 1993-07-12
- Granted: 1994-09-27
- Earliest claimed: 1993-07-12
- Assignees: American Air Liquide, Inc.
- Inventors: Benjamin Jurcik; Michael Brandt; Ronald Inman; James McAndrew
- Web page: https://patentgrep.com/patent/US5351120A

## CPC

- G01N 21/031: {Multipass arrangements}
- G01N 2021/054: {Bubble trap; Debubbling}
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

The spectrographic sample cell for the analysis of trace impurities in sample gases. The cell is provided with a gas inlet, a gas outlet and a volume for confining the sample gases for analysis. Two mirrors are provided, a first mirror proximate the gas inlet the second mirror proximate the gas outlet, the first mirror having a hole at its radial center. A conically-shaped cell profile is further provided such that the formation of vortices of sample gas is prevented in the cell upstream of or in the region where the analysis of trace impurities is to take place.

## Claims

### Claim 1

In a spectroscopic sample cell for the analysis of trace impurities in sample gases having a gas inlet, a gas outlet and a volume for confirming said sample gases for analysis, the improvements comprising:
(a) providing two mirrors, a first mirror proximate the gas inlet and a second mirror proximate the gas outlet, said first mirror having a hole at its radial center;
(b) providing a conically-shaped cell profile substantially at said gas inlet, the diverging angle of said profile being less than approximately 40.degree.; wherein the location and sizes of said mirrors and conically-shaped cell profile are such as to substantially prevent the formation of vortices in said sample cell upstream of or in the region where said analysis of trace impurities takes place.

### Claim 2 (depends on 1)

The spectroscopic sample cell of claim 1 wherein said first mirror is positioned and sized such that substantially all of the gas passing through said sample cell proceeds around said first mirror without separating into multiple stream paths.

### Claim 3 (depends on 1)

The spectroscopic sample cell of claim 1 wherein said hole in said first mirror is sized so as to allow the passage of sufficient gas to purge an area downstream of said first mirror.

### Claim 4 (depends on 1)

The spectroscopic sample cell of claim 1 wherein said cell and mirrors are substantially circular in cross-section.

### Claim 5 (depends on 4)

The spectroscopic sample cell of claim 4 wherein the hole in said first mirror is smaller than the gas inlet to said cell.

### Claim 6 (depends on 4)

The spectroscopic sample cell of claim 4 wherein said first mirror is spaced less than approximately four gas inlet diameters from the downstream end of said conically-shaped cell profile.

### Claim 7 (depends on 4)

The spectroscopic sample cell of claim 4 wherein the diameter of the first mirror is greater than the diameter of said cell at the downstream end of said conically-shaped cell profile.

### Claim 8 (depends on 4)

The spectroscopic sample cell of claim 4 wherein said first mirror is sized such that the free cell cross-sectional area at the plane at which said first mirror is located unoccupied by said first mirror is greater than the gas inlet cross-sectional area.

### Claim 9 (depends on 4)

The spectroscopic sample cell of claim 4 wherein said first mirror is approximately 4/7 of the cell diameter.

### Claim 10 (depends on 4)

The spectroscopic sample cell of claim 4 wherein said second mirror is approximately 5/7 of the cell diameter.

### Claim 11 (depends on 4)

The spectroscopic sample cell of claim 4 wherein the hole in said first mirror is approximately 1/28 of the cell diameter.

### Claim 12 (depends on 4)

The spectroscopic sample cell of claim 4 wherein said first mirror is spaced from the downstream end of said conically-shaped cell profile by a distance equal to approximately 1/4 of the cell diameter.

### Claim 13 (depends on 1)

The spectroscopic sample cell of claim 1 wherein said diverging angle of said conically-shaped cell profile is approximately 20.degree..

### Claim 14 (depends on 13)

The spectroscopic sample cell of claim 13 wherein said conically-shaped cell profile expands to approximately 50% of the cell diameter.