# US 5,350,847 A · Purification of caprolactam

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- Number: US 5,350,847 A
- Document ID: US5350847A
- Status: Granted
- Kind: A
- Application number: 08/113,081
- Filed: 1993-08-30
- Granted: 1994-09-27
- Earliest claimed: 1992-09-08
- Assignees: BASF SE
- Inventors: Hugo Fuchs; Gerald Neubauer; Claus-Ulrich Priester
- Web page: https://patentgrep.com/patent/US5350847A

## CPC

- C07D 201/16: Separation or purification
- C07D: HETEROCYCLIC COMPOUNDS (macromolecular compounds C08)

## Abstract

Caprolactam is purified by oxidative treatment in which mixtures which essentially contain the caprolactam to be purified and unsaturated lactams are treated with oxygen or an oxygen-containing gas mixture in an alkaline medium.

## Claims

### Claim 1

A process for purifying caprolactam by oxidative treatment which comprises: adding an oxide or hydroxide of an alkali metal or alkaline earth metal to a liquid mixture containing the caprolactam to be purified and unsaturated lactams to provide an alkaline medium, and thereafter passing oxygen or an oxygen-containing gas mixture through the liquid mixture.

### Claim 2 (depends on 1)

A process as defined in claim 1, wherein the alkaline medium is provided by adding sodium hydroxide, calcium oxide or magnesium oxide to the liquid mixture.

### Claim 3 (depends on 1)

A process as defined in claim 1, wherein from 0.05 to 1.0 percent by weight of the oxide of hydroxide is added to the liquid mixture based on the weight of caprolactam that is present.

### Claim 4 (depends on 1)

A process as defined in claim 1, wherein the oxidative treatment is carried out at a temperature of from 80.degree. to 100.degree. C.

### Claim 5 (depends on 1)

A process for purifying caprolactam as defined in claim 1, wherein the oxidative treatment is carried out with air.