# US 5,350,593 A · Dietary fiber derived from tapioca and process therefor

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- Number: US 5,350,593 A
- Document ID: US5350593A
- Status: Granted
- Kind: A
- Application number: 08/157,489
- Filed: 1993-11-23
- Granted: 1994-09-27
- Earliest claimed: 1991-12-23
- Assignees: National Starch and Chemical Investment Holding Corporation
- Inventors: Norman L. LaCourse; Karen Chicalo; James P. Zallie; Paul A. Altieri
- Web page: https://patentgrep.com/patent/US5350593A

## CPC

- A23L 7/135: Individual or non-extruded flakes, granules or shapes having similar size, e.g. breakfast cereals
- A21D 2/366: {Tubers, roots}
- A23L 5/25: {using enzymes}
- A23L 7/143: Cereal granules or flakes to be cooked and eaten hot, e.g. oatmeal; Reformed rice products
- A23L 7/17: by extrusion
- A23L 33/21: Addition of substantially indigestible substances, e.g. dietary fibres
- C12Y 302/01001: Alpha-amylase (3.2.1.1)
- C12Y 302/01003: Glucan 1,4-alpha-glucosidase (3.2.1.3), i.e. glucoamylase
- A23L: FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF (preservation thereof A23B)
- A21D: TREATMENT OF FLOUR OR DOUGH FOR BAKING, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS (preservation of flour or dough before baking A23B40/00; preservation of bakery products A23B45/00)
- C12Y: ENZYMES

## Abstract

Dietary fiber are derived from the tapioca pulp fiber that is a by-product of tapioca starch milling operations. The tapioca fiber may be refined through an enzymatic destarching step to provide a fiber comprising at least 70% total dietary fiber, of which at least 12% is soluble dietary fiber. The fiber may be further refined by bleaching. Acceptable foods may be prepared comprising unrefined or refined tapioca fiber.

## Claims

### Claim 1

A dietary fiber of tapioca origin, comprising on a dry solids basis, at least 70% total dietary fiber, of which at least 12% is soluble dietary fiber, and less than 15% starch, wherein the dietary fiber has a water-holding capacity of at least 2.5 and a viscosity of at least 100 B.U. in a 5% aqueous solution.

### Claim 2 (depends on 1)

The dietary fiber of claim 1, wherein the fiber is refined by bleaching with a reagent selected from the group consisting of hydrogen peroxide, sodium chlorite, sodium hypochlorite and potassium permanganate.

### Claim 3 (depends on 1)

The dietary fiber of claim 1, wherein 50% of the fiber passes through a 40 mesh screen.

### Claim 4

A process for refining tapioca pulp for use as a nutritional ingredient in nutritionally fortified processed foods, comprising the steps:
a) forming a slurry of 5 to 10%, by weight, ground tapioca pulp in an aqueous media;
b) enzymatically treating the slurry with a 1,4-alpha-D-glucosidase to depolymerize sufficient starch to yield a tapioca fiber containing less than 15% starch;
c) separating the tapioca fiber from the slurry; and
d) washing the tapioca fiber to provide a refined tapioca fiber, wherein the refined tapioca fiber contains at least 70% total dietary fiber, of which at least 12% is soluble dietary fiber, and the refined tapioca fiber has a water-holding capacity of at least 2.5 and a viscosity of at least 100 B.U. in a 5% aqueous solution.

### Claim 5 (depends on 4)

The process of claim 4, wherein the enzyme is an alpha-amylase or a glucoamylase.

### Claim 6 (depends on 5)

The process of claim 5, wherein the enzymatic treatment of a 5.10%, by weight, aqueous slurry of tapioca pulp is conducted for 3 to 5 hours at 25.degree. to 85.degree. C., employing an alpha-amylase.

### Claim 7 (depends on 6)

The process of claim 6, wherein the refined tapioca fiber comprises no more than 10%, by weight, starch and at least 75%, by weight, total dietary fiber, of which at least 15% is soluble dietary fiber.

### Claim 8 (depends on 4)

The process of claim 4, further comprising the step of drying the tapioca fiber to a moisture content of less than 15%, by weight.

### Claim 9 (depends on 8)

The process of claim 8, further comprising the step of adjusting the particle size of the tapioca fiber so that 95%, by weight, of the tapioca fiber passes through a U.S.S.S. 100 mesh screen.

### Claim 10 (depends on 4)

The process of claim 4, further comprising the step of bleaching the tapioca fiber with a reagent selected from the group consisting of hydrogen perioxide, sodium chlorite, sodium hypochlorite and potassium permanganate.

### Claim 11 (depends on 10)

The process of claim 10, wherein the reagent is sodium hypochlorite and a 5 to 10%, by weight, slurry of tapioca fiber is bleached for 5 to 6 hours at 25.degree. to 40.degree. C. at an alkaline pH.

### Claim 12 (depends on 11)

The process of claim 11, further comprising the step of drying the bleached tapioca fiber to a moisture content of less than 15%, by weight.

### Claim 13

A nutritionally-fortified, fiber-containing food comprising about 1 to 43%, by weight, of at least one dietary fiber of tapioca origin selected from the group consisting of unrefined tapioca fiber, refined tapioca fiber, comprising on a dry starch solids basis no more than 15% starch and at least 70%, by weight, total dietary fiber, of which at least 12% is soluble dietary fiber, wherein the refined tapioca fiber has a water-holding capacity of at least 2.5 and a viscosity of at least 100 B.U. in a 5% aqueous solution, and bleached, refined tapioca fiber comprising on a dry solids basis no more than 15% starch and at least 70%, by weight, total dietary fiber, of which at least 12% is soluble dietary fiber, wherein the bleached refined tapioca fiber has a water-holding capacity of at least 2.5 and a viscosity of at least 100 B.U. in a 5% aqueous solution.

### Claim 14 (depends on 13)

The food of claim 13 wherein the food is selected from the group consisting of bread and other baked goods, fried foods, breaded and coated foods and cereals.

### Claim 15 (depends on 14)

The food of claim 14, wherein one serving of the food comprises at least 4 grams of total dietary fiber, of which fiber at least 10%, by weight, is soluble dietary fiber.