# US 5,350,525 A · System and process for hydrocyclone separation of particulate solids and at least one liquid phase from a multiphase liquid mixture

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- Number: US 5,350,525 A
- Document ID: US5350525A
- Status: Granted
- Kind: A
- Application number: 07/943,845
- Filed: 1992-09-11
- Granted: 1994-09-27
- Earliest claimed: 1992-09-11
- Assignees: Conoco Specialty Products Inc.
- Inventors: Christopher K. Shaw; Phillip C. Tuckett; Bill E. Bowers
- Web page: https://patentgrep.com/patent/US5350525A

## CPC

- B04C 5/26: for series flow
- B01D 17/00: Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion (devices for separating or removing fatty or oily substances or similar floating material from water, waste water, or sewage C02F1/40; cleaning or keeping clear the surface of open water from oil or like materials E02B15/04; arrangements for separating lubricants from refrigerants F25B43/02)
- B01D 17/02: Separation of non-miscible liquids
- B01D 17/0217: {by centrifugal force}
- B01D 17/044: {by changing the pressure}
- B04C 5/24: Multiple arrangement thereof {(combination types according to other /00 groups, B04C7/00)}
- B04C: APPARATUS USING FREE VORTEX FLOW, e.g. CYCLONES ({centrifugal separation of water from steam B01D45/12;} jet mills B02C19/06; {wind sifters B07B7/00;} cyclonic type combustion apparatus F23; {vortex burners for cyclone-type combustion apparatus F23D1/02; cyclonic type combustion apparatus for gas turbines F23R3/00})
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)

## Abstract

This invention relates to a system for separating a multiphase liquid mixture into a plurality of streams. The invention has particular utility in the oil industry where particulate solids are produced with an oil/water mixture. Preferably, the mixture is first cyclonically separated to remove particulate solids from the oil and water. Then the mixture is delivered to a liquid/liquid hydrocyclone where a substantial portion of the oil is separated from the remaining mixture which now primarily comprises water. The pressure of the remaining mixture is elevated such as by a pump and is then subjected to a further cyclonic separation step to remove any remaining fine solids in the mixture.

## Claims

### Claim 1

A process for separating a multiphase liquid mixture comprising a heavy phase liquid component, a lighter phase liquid component and a particulate solids component into a plurality of separately classifiable streams, wherein the process comprises the steps of:
(a) cyclonically separating at least a portion of the mixture into a first portion and a second portion wherein the first portion comprises a relatively greater concentration of particulate solids component compared to the multiphase liquid mixture;
(b) cyclonically separating at least a portion of the second portion into an overflow and an underflow wherein the overflow comprises a relatively greater concentration of lighter phase liquid component compared to the multiphase liquid mixture;
(c) cyclonically separating a substantial portion of any remaining particulate solids from at least a portion of said underflow; and
(d) elevating the pressure of the underflow from the cyclonically separating step prior to said step of separating remaining particulate solids;
the process excluding said first portion from step (a) being further separated in equipment provided for cyclonic separation in steps (b) or (c).

### Claim 2 (depends on 1)

The process according to claim 1 further comprising separating the multiphase liquid mixture into at least a lighter phase liquid stream and a heavier phase liquid stream prior to said step (a) and providing the heavier phase liquid stream to said step (a).

### Claim 3 (depends on 1)

The process according to claim 1 further comprising the step of separating an overflow stream from said step (c) into lighter and heavier density liquid portions.

### Claim 4 (depends on 1)

The process according to claim 1 further including the step of providing the multiphase liquid mixture to a vessel prior to cyclonic separation step (a), and wherein the process further comprises sensing the fluid level in the vessel and recycling at least a portion of the higher pressure underflow from downstream of the step of elevating the pressure.

### Claim 5

A process for separating a production stream from an oil well comprising a heavier phase component, a lighter phase component and a particulate solids component into a plurality of separately classifiable streams, wherein the process comprises the steps of:
(a) separating at least a portion of the production stream into at least a lighter phase liquid stream and a heavier phase liquid stream;
(b) cyclonically separating at least a portion of the heavier phase liquid stream into a particulate solids stream and a liquid mixture stream;
(c) cyclonically separating at least a portion of the liquid mixture stream from step (b) into an overflow and an underflow wherein the overflow comprises a relatively greater concentration of lighter phase liquid component compared to such concentration in the heavier phase liquid stream produced in step (a);
(d) elevating the pressure of at least a portion of the underflow produced in step (b) to a higher pressure; and
(e) cyclonically separating particulate solids from at least a portion of the higher pressure underflow from step (c); and
(f) separating a substantially particulate solids free mixture resulting from step (e) into lighter and heavier phase liquid portions;
the process excluding said particulate solids stream from said step (b) being further separated in equipment provided for cyclonic separation in steps (c) or (e).

### Claim 6

A system for separating a multiphase liquid mixture comprising a heavy phase liquid component, a lighter phase liquid component and a particulate solids component into a plurality of separately classifiable streams, wherein the apparatus comprises:
first separation means for cyclonically separating the mixture into a first portion and a second portion wherein the first portion comprises a relatively greater concentration of particulate solids compared to the multiphase liquid mixture;
second separation means for cyclonically separating the second portion from said first separation means into an overflow and an underflow wherein the overflow comprises a greater proportion of lighter phase liquid to heavier phase liquid than the underflow;
means for elevating the pressure of the underflow; and
third separation means for cyclonically separating a substantial portion of any remaining particulate solids from the elevated pressure underflow; and
wherein said system does not include means for directing said first portion from said first separation means to either of said second or third separation means.

### Claim 7 (depends on 6)

The system according to claim 6 further comprising a gravity separation means for further separating a substantially solids free liquid mixture outletted from said third separation means into lighter and heavier phase liquid portions.

### Claim 8 (depends on 6)

The system according to claim 6 further comprising a vessel upstream of said first separation means wherein said vessel is provided with the multiphase liquid mixture therein and wherein the system further comprises means for sensing the fluid level in said vessel and means for recycling at least a portion of the elevated pressure underflow from downstream of said means for elevating the pressure.