# US 5,347,819 A · Method and apparatus for manufacturing superfluidity helium > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 5,347,819 A - Document ID: US5347819A - Status: Granted - Kind: A - Application number: 08/141,742 - Filed: 1993-10-27 - Granted: 1994-09-20 - Earliest claimed: 1992-11-05 - Assignees: Ishikawajima-Harima Heavy Industries Co., Ltd. - Inventors: Nobuyoshi Saji; Hiroshi Ohya; Hiroshi Asakura; Shunji Nagai - Web page: https://patentgrep.com/patent/US5347819A ## CPC - F25B 9/10: with several cooling stages - F25B: REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS ## Abstract Method and apparatus for manufacturing superfluidity helium (He II). The method includes the steps of (a) providing .sup.3 He gas (b) providing liquid .sup.4 He, (c) compressing the .sup.3 He gas to produce compressed .sup.3 He gas, (d) indirectly cooling the compressed .sup.3 He gas with liquid .sup.4 He to produce cryogenic .sup.3 He gas (e) adiabatically expanding the cryogenic .sup.3 He gas to produce cryogenic .sup.3 He gas having a temperature of less than about 1.18.degree. K., preferably less than 1.8.degree. K., and (f) indirectly cooling the liquid .sup.4 He with the cryogenic .sup.3 He gas produced in step (e) to produce superfluidity helium. The apparatus includes a first container for liquid helium and a second container for containing superfluidity helium, and a first line for connecting the first and second containers. A .sup.3 He refrigeration circuit is provided to cool the .sup.4 He in directly with cryogenic .sup.3 He to produce superfluidity helium. The method and apparatus enables superfluidity helium to be produced without the use of a large vacuum pump whose lubricants might contaminate the superfluidity helium. The method and apparatus also allow superfluidity helium at or near standard pressure to be easily produced and maintained. ## Claims ### Claim 1 A method for producing superfluidity helium comprising the steps of: (a) providing cryogenic .sup.3 He; (b) providing liquid .sup.4 He in a first container; (c) compressing the cryogenic .sup.3 He to produce compressed .sup.3 He; (d) indirectly cooling the compressed .sup.3 He with liquid .sup.4 He in said first container to produce cryogenic .sup.3 He; (e) adiabatically expanding the cryogenic .sup.3 He to produce cryogenic .sup.3 He having a temperature of less than 2.18.degree. K.; and (f) indirectly cooling the liquid .sup.4 He in a second container with the cryogenic .sup.3 He produced by step (e) to produce superfluidity helium. ### Claim 2 (depends on 1) A method according to claim 1, further comprising the step of (g) maintaining said superfluidity .sup.4 He substantially at a pressure of 1 atm. ### Claim 3 (depends on 1) A method according to claim 1, wherein, said cryogenic .sup.3 He produced in step (e) has a temperature of less than about 1.8.degree. K. ### Claim 4 (depends on 1) A method according to claim 1, wherein, in step (e), said cooled cryogenic .sup.3 He is adiabatically expanded to a pressure of less than about 200 Torr. ### Claim 5 (depends on 1) A method according to claim 1, further comprising the step, after said step (d) , of indirectly cooling said cooled .sup.3 He with .sup.3 He recycled after being used to produce superfluidity .sup.4 He in said step (f). ### Claim 6 (depends on 5) A method according to claim 5, wherein, after step (d) and before said step of indirectly cooling, the steps (c) and (d) are repeated, so that said cooled, cryogenic .sup.3 He produced by step (d) is further compressed according to step (c) and a resulting compressed gas is further cooled according to step (d). ### Claim 7 (depends on 6) A method according to claim 6, further comprising the step of maintaining the second container at a pressure of substantially 1 atm. ### Claim 8 (depends on 1) A method according to claim 1, wherein said step (b) comprises producing the liquid .sup.4 He using a Claude cycle process. ### Claim 9 (depends on 1) A method according to claim 1 wherein said .sup.3 He comprises a mixture of .sup.3 He and .sup.4 He. ### Claim 10 (depends on 1) A method according to claim 1, wherein said cryogenic .sup.3 He of step (f) is recycled, after step (f), to step (c) to form a .sup.3 He cycle wherein steps (c), (d), (e), and (f) are cyclically repeated. ### Claim 11 (depends on 1) A method according to claim 1, wherein, after step (d) and before step (f), steps (c) and (d) are repeated, so that said cryogenic .sup.3 He produced by step (d) is further compressed according to step (c) and a resulting compressed gas is further cooled according to step (d). ### Claim 12 (depends on 11) A method according to claim 11, further comprising the step of maintaining the second container at a pressure of substantially 1 atm. ### Claim 13 (depends on 1) A method according to claim 1, further comprising the step of maintaining the second container at a pressure of substantially 1 atm. ### Claim 14 (depends on 1) A method according to claim 1, wherein step (b) further comprises providing liquid .sup.4 He in a third container, and said method further comprises the steps of expanding liquid .sup.4 He from the third container to form expanded liquid .sup.4 He, and providing the expanded liquid .sup.4 He to the first container. ### Claim 15 (depends on 14) A method according to claim 14, further comprising the step of maintaining said second container at a pressure of about 0.4 atm. ### Claim 16 (depends on 14) A method according to claim 14, wherein said step (b) further comprises providing a fourth container, and wherein said method further comprises the steps of: expanding liquid .sup.4 He from the first container to produce expanded liquid .sup.4 He, and providing the expanded liquid .sup.4 He from the first container to the fourth container; the step, after step (d) and before step (e), of indirectly cooling said cryogenic .sup.3 He produced by step (d) with liquid .sup.4 He in the fourth container to produce further cooled cryogenic .sup.4 He gas; recycling .sup.3 He used in step (f) to step (c), and cyclically repeating steps (c), (d), (e) and (f); and indirectly cooling .sup.3 He recycled from step (f) with further cooled cryogenic .sup.3 He produced by indirect cooling in the fourth container. ### Claim 17 An apparatus for producing superfluidity helium, comprising: a first container for storing liquid .sup.4 He; a second container for storing superfluidity .sup.4 He; a first line connecting the first and second containers; and a .sup.3 He refrigeration circuit including (a) a first compressor for compressing .sup.3 He, (b) a first heat exchanger, disposed downstream of the first compressor and located in the first container, for indirectly cooling compressed .sup.3 He from the first compressor with liquid .sup.4 He in the first container to produce cooled, compressed .sup.3 He, (c) means, disposed downstream of the first heat exchanger, for adiabatically expanding the cooled, compressed .sup.3 He from the first heat exchanger to produce a cryogenic .sup.3 He, and (d) a second heat exchanger, disposed downstream of the first heat exchanger and located in the second container, for indirectly cooling liquid .sup.4 He in the second container with the cryogenic .sup.3 He to produce superfluidity .sup.4 He, and (e) a second line connecting the second heat exchanger with the first compressor to form a .sup.3 He refrigeration circuit. ### Claim 18 (depends on 17) An apparatus according to claim 17, where said means (c) comprises a JT valve. ### Claim 19 (depends on 17) An apparatus according to claim 17, wherein said .sup.3 He refrigeration circuit further comprises: (f) a second compressor, disposed between the first heat exchanger and the means for adiabatically expanding, to further compress said cooled compressed .sup.3 He; (g) a third heat exchanger, disposed between the second compressor and the means for adiabatically expanding and located in the first container, for further cooling the cooled, compressed .sup.3 He; and (h) a fourth heat exchanger, disposed between the third heat exchanger and the means for adiabatically expanding, for cooling .sup.3 He in the second line indirectly with cooled, compressed .sup.3 He from the third heat exchanger. ### Claim 20 (depends on 19) An apparatus according to claim 19, further comprising: a third container for containing .sup.4 He; a third line connecting the third container with said first container; and means, disposed in the third line, for expanding liquid .sup.4 He from the third container and introducing expanded liquid .sup.4 He into said first container. ### Claim 21 (depends on 17) An apparatus according to claim 17, further comprising: (h) an additional heat exchanger disposed between the first heat exchanger and the means for adiabatically expanding, for cooling .sup.3 He in the second line indirectly with cooled, compressed .sup.3 He from the first heat exchanger. ### Claim 22 (depends on 21) An apparatus according to claim 21, further comprising: a third container for containing .sup.4 He; a line connecting the third container with said first container; and means for expanding liquid .sup.4 He from the third container and introducing expanded liquid .sup.4 He into said first container. ### Claim 23 (depends on 22) An apparatus according to claim 22, further comprising: a fourth container for containing liquid .sup.4 He; a fourth line connecting said first container with the fourth container; and means, disposed in the fourth line, for expanding liquid .sup.4 He from the first container and introducing expanded liquid .sup.4 He into the fourth container; and wherein said .sup.3 He refrigeration circuit further comprises (g) a third heat exchanger disposed in the .sup.3 He circuit between the first heat exchanger and the additional heat exchanger, and located in the fourth container, for further cooling cooled, compressed .sup.3 He from the first heat exchanger with liquid .sup.4 He in the fourth container. ### Claim 24 (depends on 17) An apparatus according to claim 17, further comprising: a third container for containing .sup.4 He; a third line connecting the first and third containers; and means, disposed in the third line, for adiabatically expanding liquid .sup.4 He from the third container and introducing expanded liquid .sup.4 He into said first container. ### Claim 25 (depends on 17) An apparatus according to claim 17, further comprising means for containing an object to be cooled by said superfluidity helium within said second container. ### Claim 26 (depends on 25) An apparatus according to claim 25, wherein said object is a superconducting electromagnet. ### Claim 27 (depends on 26) An apparatus according to claim 26, wherein said object is an electromagnet. ### Claim 28 (depends on 17) An apparatus according to claim 17, further comprising means for conducting superfluidity helium from said second container to an object to be cooled by said superfluidity helium. ### Claim 29 (depends on 17) An apparatus according to claim 17, wherein the first compressor is a centrifugal gas bearing compressor. ### Claim 30 (depends on 17) An apparatus according to claim 17, wherein the first compressor is a centrifugal magnetic bearing compressor.