# US 5,346,575 A · Glass fiber insulation and process

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- Number: US 5,346,575 A
- Document ID: US5346575A
- Status: Granted
- Kind: A
- Application number: 08/026,651
- Filed: 1993-03-05
- Granted: 1994-09-13
- Earliest claimed: 1991-09-30
- Assignees: Monsanto Company
- Inventors: Edward J. Griffith; Toan M. Ngo
- Web page: https://patentgrep.com/patent/US5346575A

## CPC

- C03C 25/42: Coatings containing inorganic materials
- Y10S 428/92: Fire or heat protection feature
- Y10T 428/24826: Spot bonds connect components
- Y10T 428/2905: Plural and with bonded intersections only
- Y10T 428/2933: Coated or with bond, impregnation or core
- C03C: CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- Y10S: TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10T: TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION

## Abstract

There is disclosed novel glass fiber particularly useful for preparing formed insulating articles having on the surface of the fibers an amorphous aluminum phosphate polymer wherein the polymer resiliently tacks the glass fibers together so as to provide regain of shape after deformation of the fibers as by compression. Also disclosed is a process for preparing glass fiber articles wherein the fibers are contacted with an ionic polymer which is then dehydrated to form an amorphous non-hygroscopic polymer.

## Claims

### Claim 1

A process for preparing a form retaining insulating body of glass fibers comprising applying to the fibers a tacking agent comprising an aqueous acid aluminum phosphate solution containing a molar ratio of Al.sub.2 O.sub.3 to P.sub.2 O.sub.5 of less than 1, shaping said body and then removing water from said tacking agent to form an amorphous, water insoluble, non-hygroscopic polymer whereby the glass fibers of the body form are resilently bonded together.

### Claim 2 (depends on 1)

A process of claim 1 wherein water is removed by heating the fibers by means selected from the group consisting of electric or gas fired ovens, microwave or infrared radiation.

### Claim 3 (depends on 1)

A process of claim 1 wherein the ratio of Al.sub.2 O.sub.3 to P.sub.2 O.sub.5 is in the range of from about 1:2 to about 1:3.

### Claim 4

A process for preparing a loose mass of glass fibers which comprises applying to the fibers a tacking agent comprising an aqueous acid aluminum phosphate solution containing a molar ratio of Al.sub.2 O.sub.3 to P.sub.2 O.sub.5 of from 1:2 to 1:4, and then removing water to form an amorphous, water insoluble,non-hygroscopic polymer.

### Claim 5 (depends on 4)

A process of claim 4 wherein the ratio of Al.sub.2 O.sub.3 to P.sub.2 O.sub.5 is about 1:3.

### Claim 6 (depends on 4)

A process of claim 4 wherein the water is removed by heating the fibers by means selected from the group consisting of electric ovens, microwave or infrared radiation.