# US 5,345,774 A · Method and apparatus for zero emissions testing of a refrigerant in a closed system > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 5,345,774 A - Document ID: US5345774A - Status: Granted - Kind: A - Application number: 08/011,874 - Filed: 1993-02-01 - Granted: 1994-09-13 - Earliest claimed: 1993-02-01 - Assignees: Carrier Corporation - Inventors: Gordon L. Mount - Web page: https://patentgrep.com/patent/US5345774A ## CPC - G01N 1/2035: {by deviating part of a fluid stream, e.g. by drawing-off or tapping} - G01M 3/226: {for containers, e.g. radiators} - G01N 2001/2064: {using a by-pass loop} - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) - G01M: TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR ## Abstract An external fluid circuit capable of being connected between service valves provided on a closed system containing a refrigerant. The external fluid circuit is provided with a testing tube and testing tube holder. A flow meter and flow regulator are connected in series in the external fluid circuit. The flow meter is provided with a transparent chamber containing a float indicator member to indicate when a desired rate of refrigerant flow through the circuit has been achieved. A three-way toggle valve is provided between the flow meter and testing tube holder allowing the refrigerant to be directed through the testing tube or through a bypass loop. A hand-held compressor downstream of the testing tube holder induces sufficient flow pressure difference where there is insufficient system pressure to cause proper flow through the external fluid circuit. ## Claims ### Claim 1 Apparatus for testing for contaminates in a refrigerant in a closed system having a first and a second isolation valve, the apparatus comprising: an external fluid circuit capable of being connected between the isolation valves allowing an amount of the refrigerant from the closed system to flow therethrough in a predetermined direction from the first to the second isolation valve when the isolation valves are open; the external circuit including detecting means for identifying contaminants within the refrigerant as the refrigerant flows therethrough, said detecting means being in series between said isolation valves and having an upstream end and a downstream end relative to the direction of refrigerant flow, flow meter means in series with said detecting means for determining the rate of flow of said refrigerant flowing through said external fluid circuit, said flow meter means being connected upstream of said detecting means; flow regulator means for adjusting the flow of refrigerant through said external fluid circuit to a desired rate, said flow regulator means being upstream of said flow meter means; and three-way valve means for directing the flow of refrigerant through the circuit, said three-way valve means having an inlet port, a first outlet port, and a second outlet port, said inlet port being connected to receive the refrigerant from said flow meter means, and said second outlet port being connected to the upstream end of said detecting means; and a bypass line coupled to the first outlet port of the three way valve means and to a point downstream of the detecting means; whereby when the isolation valves are open, the flow of refrigerant through said external fluid circuit can be first directed through said bypass line to bypass said detecting means when said three-way valve means has its first outlet port open and its second outlet port closed, thus allowing the flow through the circuit to be adjusted to the desired rate of flow by said flow regulator means, and can then be directed to flow through said detecting means by actuating said valve means so that its first outlet port is closed and its second outlet port is open, thus allowing said detecting means to identify contaminants in the refrigerant prior to the refrigerant being returned to the closed system. ### Claim 2 (depends on 1) The apparatus according to claim 1 further including compressor means having a suction line and a discharge line, the suction line being coupled to the bypass line and to the downstream end of said detecting means, the discharge line of said compressor means being coupled to the second isolation valve. ### Claim 3 (depends on 2) The apparatus according to claim 2 wherein said compressor means includes a hand-held compressor. ### Claim 4 (depends on 3) The method according to claim 3 including the further step of providing the external fluid circuit with three-way valve means for selectively directing the refrigerant flow through the bypass loop and the detecting loop. ### Claim 5 (depends on 1) The apparatus according to claim 1 wherein said flow meter means includes a transparent flow indicating chamber held vertically during operation and having a free-floating flow-responsive member contained therein and a flow line thereon to indicate the desired rate of flow. ### Claim 6 (depends on 5) The apparatus according to claim 5 wherein said flow regulator means includes a needle valve capable of adjusting the flow of refrigerant into said flow indicating chamber at an increasing rate to cause the free-floating member to reach the flow line thereby indicating that the desired rate of flow has been attained. ### Claim 7 (depends on 1) The apparatus according to claim 1 wherein said detecting means includes a testing tube and a testing tube holder, said testing tube holder including: a generally elongate transparent container having oppositely disposed open ends, one of said open ends being an open upstream end and the other one of said open ends being an open downstream end, said container being adapted to removably contain therein said testing tube, a first coupling member connected to said open upstream end and having therein a passage in fluid communication with said container; a first sealing means being adapted for providing a fluid tight fit between said first coupling member and said testing tube; a second coupling member connected to said open downstream end and having therein a passage in fluid communication with said container; and a second sealing means being adapted for providing a fluid tight fit between said second coupling member and said container; said testing tube including: a single elongate tube member made of a generally transparent material and having oppositely disposed breakable ends, said ends of said tube member can be broken open to define respectively an upstream opening and a downstream opening; an oil removal section adjacent said upstream end of said tube; a first contaminant-indicating substance disposed in said tube member downstream of said oil removal section and adapted to remove and indicate the presence of water in the refrigerant flowing therethrough; a second contaminant-indicating substance disposed downstream of said first contaminant indicating substance and being adapted to indicate the presence of acid in the refrigerant flowing therethrough; and means disposed between said first and second contaminant-indicating substances for preventing migrational action therebetween. ### Claim 8 (depends on 7) The apparatus according to claim 7 wherein said means disposed between said first and second contaminant-indicating substances includes a pair of fluid permeable partitions separated by screen means. ### Claim 9 (depends on 7) The apparatus according to claim 7 wherein said first contaminant-indicating substance includes cobaltous chloride on a silica sand base. ### Claim 10 (depends on 7) The apparatus according to claim 7 wherein said second contaminant-indicating substance includes bromophenol blue on a glycerol film coating a silica sand base. ### Claim 11 A method for detecting the presence and amount of contaminants in a refrigerant, subject to contain oil, moisture and acid, flowing in a closed system having a first and a second isolation valve without causing discharge of the refrigerant from the closed system into the atmosphere, the method comprising the steps of: removable connecting between said isolation valves an external fluid circuit having in parallel a bypass loop and a detecting loop allowing a limited amount of refrigerant from the closed system to flow through the circuit in a predetermined direction from the first isolation valve to the second isolation valve; providing the external fluid circuit with a hand-held compressor pump to induce refrigerant flow through the circuit; providing in series in the detecting loop of the external fluid circuit a testing tube capable of allowing the refrigerant flow to pass therethrough to detect contaminants in the refrigerant; opening the isolation valves to allow the refrigerant to flow into the external fluid circuit through the bypass loop and back into the closed system through the second isolation valve; regulating the flow of refrigerant through the external fluid circuit to a desired rate of flow; directing the regulated flow at said desired rate to the detecting loop; removing any oil present in the directed flow of refrigerant passing through the testing tube; determining the amount of water present in the directed flow of refrigerant passing through the testing tube; determining the amount of acid present in the directed flow of refrigerant passing through the testing tube; and returning said directed flow to the closed system through the second isolation valve. ### Claim 12 (depends on 11) The method according to claim 11 wherein said compressor is disposed downstream of said detecting loop. ### Claim 13 A light-weight portable apparatus for testing for contaminates in a refrigerant in a closed system having a first and a second isolation valve, said apparatus comprising: an external fluid circuit capable of being connected between the isolation valves to allow an amount of the refrigerant from the closed system to flow therethrough in a predetermined direction from the first to the second isolation valve when the isolation valves are open, said external circuit including; detecting means for identifying contaminants within the refrigerant as tile refrigerant flows therethrough, said detecting means being engaged with the fluid circuit and having an upstream end and a downstream end relative to the direction of refrigerant flow; flow regulator means for controlling the flow of refrigerant through said external fluid circuit to a desired rate; and flow meter means fluidly engaged with said detecting means for determining the rate of flow of said refrigerant flowing through said external fluid circuit. ### Claim 14 (depends on 13) The apparatus according to claim 13 wherein said flow meter means is connected upstream of said detecting means. ### Claim 15 (depends on 13) The apparatus according to claim 13 wherein said flow regulator means is positioned upstream of said flow meter means. ### Claim 16 (depends on 13) The apparatus according to claim 13 further including three-way valve means for directing the flow of refrigerant through the circuit, said three-way valve means having an inlet port, a first outlet port, and a second outlet port, said inlet port being connected to receive the refrigerant from said flow meter means, and said second outlet port being connected to the upstream end of said detecting means; and a bypass line coupled at one end to the first outlet port of the three-way valve means and at the other end back into the circuit at a predetermined point downstream of the detecting means so that when the isolation valves are open, the flow of refrigerant through said external fluid circuit can be directed through said bypass line to circumvent said detecting means when said three-way valve means has its first outlet port open and its second outlet port closed. ### Claim 17 (depends on 16) The apparatus according to claim 16 wherein the flow of refrigerant is directed to flow through said detecting means by actuating said valve means so that its first outlet port is closed and its second outlet port is open thereby allowing said detecting means to identify contaminants in the refrigerant prior to the refrigerant being returned to the closed system. ### Claim 18 (depends on 16) The apparatus according to claim 16 further including compressor means having a suction line and a discharge line wherein said suction line is coupled into said bypass line and the downstream end of said detecting means, and said discharge line of said compressor means is coupled into the second isolation valve. ### Claim 19 (depends on 18) The apparatus according to claim 18 wherein said compressor means includes a hand-held compressor. ### Claim 20 (depends on 13) The apparatus according to claim 13 wherein said flow meter means includes a transparent flow indicating chamber positioned vertically during operation, the chamber having a free-floating flow-responsive member contained therein and a flow line thereon to indicate the desired rate of flow. ### Claim 21 (depends on 20) The apparatus according to claim 20 wherein said flow regulator means is adjustable and includes a needle valve capable of adjusting the flow of refrigerant into said flow indicating chamber at an increasing rate to cause the free-floating member to reach the flow line thereby indicating that the desired rate of flow has been attained. ### Claim 22 (depends on 13) The apparatus according to claim 13 wherein said detecting means includes a testing tube and a testing tube holder, said testing tube holder including: a generally elongate transparent container having oppositely disposed open ends, one of said open ends being an open upstream end and the other one of said open ends being an open downstream end, said container being adapted to removably contain therein said testing tube; a first coupling member connected to said open upstream end and having therein a passage in fluid communication with said container; a first sealing means being adapted for providing a fluid-tight fit between said first coupling member and said testing tube; a second coupling member connected to said open downstream end and having therein a passage in fluid communication with said container; and a second sealing means being adapted for providing a fluid-tight fit between said second coupling member and said container. ### Claim 23 (depends on 22) The apparatus according to claim 22 wherein said testing tube includes: a single elongate tube member made of a generally transparent material and having oppositely disposed breakable ends, said ends of said tube member capable of breaking open to define, respectively, an upstream opening and a downstream opening; an oil removal section adjacent said upstream end of the tube member; a first contaminant-indicating substance being disposed in the tube member downstream of said oil removal section and adapted to indicate and remove the presence of water in the refrigerant flowing therethrough; a second contaminant-indicating substance being disposed downstream of said first contaminant-indicating substance and adapted to indicate the presence of acid in the refrigerant flowing therethrough; and means disposed between said first and second contaminant-indicating substances for preventing migrational action therebetween. ### Claim 24 (depends on 23) The apparatus according to claim 23 wherein said means disposed between said first and second contaminant-indicating substances includes a pair of fluid permeable partitions separated by screen means. ### Claim 25 (depends on 23) The apparatus according to claim 23 wherein said first contaminant-indicating substance includes cobaltous chloride on a silica sand base. ### Claim 26 (depends on 23) The apparatus according to claim 23 wherein said second contaminant-indicating substance includes bromophenol blue on a glycerol film coating a silica sand base.