# US 5,345,066 A · Device for heating substances under the development of high pressures in a microwave field

> Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt

- Number: US 5,345,066 A
- Document ID: US5345066A
- Status: Granted
- Kind: A
- Application number: 07/852,528
- Filed: 1992-03-17
- Granted: 1994-09-06
- Earliest claimed: 1991-03-18
- Inventors: Gunter Knapp; Franz Panholzer
- Web page: https://patentgrep.com/patent/US5345066A

## CPC

- B01J 3/002: {Component parts of these vessels not mentioned in B01J3/004, B01J3/006, B01J3/02 - B01J3/08; Measures taken in conjunction with the process to be carried out, e.g. safety measures}
- B01J 19/126: {Microwaves}
- B01L 7/02: Water baths; Sand baths; Air baths
- G01N 1/44: Sample treatment involving radiation, e.g. heat
- H05B 6/64: Heating using microwaves {(containers, packaging elements or packages specially adapted to be heated by microwaves B65D81/3446)}
- B01J 2219/00094: Jackets
- B01J 2219/1209: Features relating to the reactor or vessel
- B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01L: CHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- H05B: ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL

## Abstract

A device for heating substances under the development of high pressures in a microwave field is disclosed. Those parts of the device lying in the microwave field comprise material transparent to microwaves. The device comprises a pressure-resistant cylindrically shaped outer container and a cylindrically shaped inner container disposed inside the outer container. Both the inner and outer container is provided with a cover or a cap for closure thereof. An interspace is provided between an inner jacket surface of the outer container and an outer jacket surface of the inner container, which space is connected with a space outside the device via connecting channels. The interspace preferably contains a cooling media which is transported to and from the interspace and outer space via the connecting channels.

## Claims

### Claim 1

A device for heating substances under the development of high pressures in a microwave field, comprising
a pressure-resistant cylindrically shaped outer container comprising a pot-like vessel and having an opening, an outer cap detachably connected to said pot-like vessel via an outer/inner engaging connection so as to open or close said pot-like vessel,
a cylindrically shaped inner container disposed in an inner portion of said pot-like vessel, said inner container comprising a front-face opening, a cover for said front-face opening, and sealing means for closing the inner container tightly,
a pressing plunger structured and arranged to act upon the outside of the cover to seal said inner container, said pressing plunger being elastically braced against said outer container, wherein those parts of the device lying in the microwave field comprise a material transparent to microwaves,
an interspace located between an inner jacket surface of said outer container and an outer jacket surface of said inner container, said interspace containing a cooling media,
said outer container further comprising connecting channels running from an outer surface of said outer container to said interspace, said connecting channels adapted to allow said cooling media to flow between said interspace and a space outside said device.

### Claim 2 (depends on 1)

The device of claim 1, wherein the distance from said inner jacket surface of said outer container to said outer jacket surface of said inner container is from about 1/50 to about 1/2 of the outer diameter of the inner container.

### Claim 3 (depends on 2)

The device of claim 2, further comprising at least one radial spacer disposed in the vicinity of said opening of said inner container between said inner container and said outer container.

### Claim 4 (depends on 3)

The device of claim 3, wherein said at least one radial spacer is disposed between said cover of said inner container and said outer container.

### Claim 5 (depends on 1)

The device of claim 1, wherein said cooling media is a gas or liquid which substantially does not absorb microwaves.

### Claim 6 (depends on 1)

The device of claim 1, wherein said cooling media is air.