# US 5,344,480 A · Pressurizing with and recovering helium

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- Number: US 5,344,480 A
- Document ID: US5344480A
- Status: Granted
- Kind: A
- Application number: 08/049,776
- Filed: 1993-04-21
- Granted: 1994-09-06
- Earliest claimed: 1992-05-05
- Assignees: Praxair Technology, Inc.
- Inventors: Thomas R. Schulte; Carl J. Heim; Vladimir T. Gorjaczkowski; Salvatore Giglia
- Web page: https://patentgrep.com/patent/US5344480A

## CPC

- G01M 3/202: {using mass spectrometer detection systems}
- B01D 53/226: {in serial connexion}
- B01D 53/229: {Integrated processes (Diffusion and at least one other process, e.g. adsorption, absorption)}
- C01B 23/00: Noble gases; Compounds thereof (liquefying F25J {; noble gases obtained by rectification F25J3/028})
- G01M: TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- C01B: NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; {METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C}

## Abstract

A process and system for pressurizing a vessel for integrity testing with gas comprising helium, recovering the gas comprising helium, and purifying the gas comprising helium for reuse. The process for purifying the gas stream comprising helium comprises drying the gas stream; separating the dried gas stream in a membrane separator stage into a helium-enriched permeate product stream and a helium-depleted raffinate stream; recovering helium in the raffinate stream in a membrane stripper stage thereby producing a purge stream; and purging water from the dryer with the purge stream.

## Claims

### Claim 1

A process for purifying a gas stream comprising helium and air constituents, said process comprising:
(a) drying the gas stream in a fluid stream dryer;
(b) separating the dried gas stream in a membrane separator stage into a helium-enriched permeate product stream and a helium-depleted raffinate stream;
(c) recovering helium in said raffinate stream in a membrane stripper stage thereby producing a purge stream; and
(d) purging water from said dryer with said purge stream.

### Claim 2 (depends on 1)

The process as in claim 1 further comprising compressing said gas stream comprising helium prior to drying said gas stream.

### Claim 3 (depends on 2)

The process as in claim 2 wherein said recovering helium from the raffinate stream in said membrane stripper stage comprises producing a permeate stream as a purge stream, and said process further comprises adding the purge stream after it has purged water from said dryer into the stream of gas comprising helium prior to compressing said gas stream.

### Claim 4 (depends on 2)

The process as in claim 2 wherein said recovering helium from the raffinate stream in said membrane stripper stage comprises producing a raffinate stream as a purge stream, producing a helium-enriched permeate stream, and adding the helium-enriched permeate stream into the stream of gas comprising helium prior to compressing said gas stream.

### Claim 5 (depends on 1)

The process as in claim 1 wherein said dryer comprises a membrane dryer and the purge stream sweeps the permeate side of the membrane dryer to maintain permeation of moisture from the gas stream.

### Claim 6 (depends on 1)

The process as in claim 1 wherein said dryer comprises at least two switchable adsorbent beds, one of said beds serving to dry the gas stream, while the other of said beds is regenerated or desorbed of water by the purge stream.

### Claim 7 (depends on 1)

The process as in claim 1 for purifying gas comprising helium and air constituents, said gas entering or contained in a tank for supplying gas comprising helium to a vessel for integrity testing thereof.

### Claim 8

A helium purification system for purifying a gas stream comprising helium and air constituents including water, said system comprising:
(a) a fluid stream dryer having:
a port for receiving a moisture-rich stream;
a port for discharging a moisture-depleted stream;
a port for receiving a moisture-depleted purge stream for purging moisture from said dryer; and
a port for discharging a moisture-enriched purge stream; and
(b) a membrane separator having:
an inlet for receiving a gas stream comprising helium, said inlet communicating with said dryer port for discharging said moisture-depleted stream;
a permeate outlet for discharging a helium-enriched permeate stream; and
a raffinate outlet for discharging a helium-depleted raffinate stream; and
(c) a membrane stripper having:
an inlet communicating with the raffinate outlet of said membrane separator; and
an outlet for discharging a purge stream, said outlet communicating with said dryer port for receiving said moisture-depleted purge stream.

### Claim 9 (depends on 8)

The system as in claim 8 further comprising compressing means, said compressing means having an inlet for receiving said gas stream comprising helium and air constituents including water and an outlet communicating with said dryer port for receiving said moisture-rich stream.

### Claim 10 (depends on 9)

The system as in claim 9 wherein said dryer port for discharging said moisture-enriched purge stream communicates with said compressing means inlet, said membrane stripper outlet for discharging said purge stream comprises a permeate outlet, and said membrane stripper further comprises a raffinate outlet communicating externally of said system.

### Claim 11 (depends on 9)

The system as in claim 9 wherein said dryer port for discharging said moisture-enriched purge stream communicates externally of said system, said membrane stripper outlet for discharging said purge stream comprises a raffinate outlet, and said membrane stripper further comprises a permeate outlet communicating with said compressing means inlet.

### Claim 12 (depends on 9)

The system as in claim 9 wherein said dryer comprises a membrane dryer and said port for receiving said moisture-depleted purge stream and said port for discharging said moisture-enriched purge stream comprise means for sweeping the permeate side of the membrane dryer to maintain a rate of permeation of moisture from the moisture-rich stream.

### Claim 13 (depends on 9)

The system as in claim 9 wherein said dryer comprises at least two switchable adsorbent beds, one of said beds serving to dry the moisture-rich stream during its adsorbing period, while the other of said beds is regenerated or desorbed of water during its desorbing period by said moisture-depleted purge stream.