# US 5,344,122 A · Tubular rod and device for sampling and analyzing fumes and apparatus including such device

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- Number: US 5,344,122 A
- Document ID: US5344122A
- Status: Granted
- Kind: A
- Application number: 07/930,381
- Filed: 1992-09-08
- Granted: 1994-09-06
- Earliest claimed: 1991-01-15
- Assignees: L'Air Liquide, Societe Anonyme pour l'Etude et l'Exploitation des Procedes Georges Claude
- Inventors: Jean-Claude Vuillermoz; Nicolas Perrin; Michel Devaux
- Web page: https://patentgrep.com/patent/US5344122A

## CPC

- C21C 5/5217: {equipped with burners or devices for injecting gas, i.e. oxygen, or pulverulent materials into the furnace}
- F27D 9/00: Cooling of furnaces or of charges therein (casings, linings, walls or roofs incorporating cooling arrangements F27D1/12)
- F27D 17/20: Arrangements for treatment or cleaning of waste gases
- F27D 17/304: {specially adapted for electric arc furnaces}
- F27D 21/00: Arrangement of monitoring devices; Arrangement of safety devices
- G01N 1/2258: {in a stack or chimney}
- G01N 2001/2282: {with cooling means}
- Y02P 10/20: Recycling
- C21C: PROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
- F27D: DETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)
- Y02P: CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS

## Abstract

The tubular rod (7) for sampling, mounted in a duct for the evacuation of fumes for example from a heat treatment or a melting furnace, includes an extractor tube (8) extending in a closed sleeve (9) comprising an inlet (11) and an outlet (12) of cooling fluid, the extractor tube having an end part opening outside the sleeve by means of an opening (10) for sampling fumes and a connecting part (14) extending outside the sleeve for connection to a circuit of analysis including a suction pump. The opening (10) is advantageously directed in counter-current with respect to the direction of circulation (F) of the fumes (11). Application such as for process control in an electrical furnace for the production of steel with injection of oxygenated gas.

## Claims

### Claim 1

A fume sampling unit comprising a casing including a main part having an axis and comprising means for connection to a source of a cooling fluid, an extractor tube having an end part extending in the casing and opening outwardly of the casing by a fume inlet opening, and an intermediate tubular member housed in the casing and surrounding the end part of the extractor tube, the intermediate tubular member being spaced from the casing and from the extractor tube to define with the casing and with the extractor tube an inner circuit for the cooling fluid.

### Claim 2

Device for sampling and analyzing fumes in a duct disposed for the evacuation of fumes, comprising at least one tubular rod mounted on said duct and having a casing including a main part having an axis and comprising means for connection to a source of cooling fluid, an extractor tube having an end part extending in the casing and opening outwardly of the casing by a fume inlet opening and a connection part extending outside the main part of the casing and wherein the fume inlet opening of said extractor tube leads to the trajectory of the fumes inside the duct, and an intermediate tubular member housed in the casing and surrounding the end part of the extractor tube, the intermediate tubular member being spaced from the casing and from the extractor tube to define with the casing and with the extractor tube an inner circuit for the cooling fluid.

### Claim 3

Apparatus for the production of steel or ferro-alloys comprising an arc furnace provided with a duct for the evacuation of fumes and a device for sampling and analyzing said fumes ,said device comprising at least one tubular rod mounted on said duct and having a casing including a main part having an axis and comprising means for connection to a source of cooling fluid, an extractor tube having an end part extending in the casing and opening outwardly of the casing by a fume inlet opening and a connection part extending outside the main part of the casing and wherein the fume inlet opening of said extractor tube leads to the trajectory of the fumes inside the duct, and an intermediate tubular member housed in the casing and surrounding the end part of the extractor tube, the intermediate tubular member being spaced from the casing and from the extractor tube to define with the casing and with the extractor tube an inner circuit for the cooling fluid.

### Claim 4

Apparatus for the production of steel or ferro-alloys comprising an arc furnace having a displaceable vault including a fumes duct section and a fumes exhaust duct having an inlet end, said fumes duct section positioned, in operating the arc furnace, in registration with the inlet end of the fumes exhaust duct defining an intermediary space therebetween, and a fume sampling unit mounted on the inlet end of the fumes exhaust duct and including a tubular casing having a lateral wall and opposite inlet and outlet for a cooling fluid, an extractor tube having an end part extending in the casing and opening outwardly of the lateral wall of the casing by a fume inlet opening, the casing positioned within the intermediary space with the opening of the extractor tube facing the inlet end of the fume exhaust duct.

### Claim 5 (depends on 1)

The fume sampling unit according to claim 1 wherein the fume inlet opening is substantially coaxial to the axis of the main part of the casing.

### Claim 6 (depends on 1)

The fume sampling unit according to claim 1 wherein the fume inlet opening is substantially perpendicular to the axis of the main part of the casing.

### Claim 7 (depends on 6)

The fume sampling unit according to claim 6 wherein the end part of the extractor tube is elbow shaped.

### Claim 8 (depends on 7)

The fume sampling unit according to claim 7 wherein the elbow shaped end part has a radius which is three time the diameter of the extractor tube.

### Claim 9 (depends on 7)

The fine sampling unit according to claim 7 wherein the casing has an end part shaped as the end part of the extractor tube.

### Claim 10 (depends on 2)

Device according to claim 2 wherein the fume inlet opening of said extractor tube is substantially perpendicular to the axis of said main part of said casing, and wherein the tubular rod is oriented in the duct so that the fume inlet opening of the extractor tube is counter-current to the direction of circulation of the fumes.

### Claim 11 (depends on 10)

Device according to claim 10 wherein at least one suction means is connected to the extractor tube of the tubular rod and to a system of analysis.

### Claim 12 (depends on 11)

Device according to claim 11 wherein the system of analysis comprises a water analyzer.

### Claim 13

Device according to claim wherein the tubular rod is connected to the water analyzer by means of a circuit including insulation and heating means.

### Claim 14 (depends on 11)

Device according to claim 11 and further comprising means for injecting an unplugging gas in the extractor tube of the tubular rod.

### Claim 15 (depends on 11)

Device according to claim 11 wherein at least one temperature probe in the trajectory of the fumes is coupled to the system of analysis.

### Claim 16 (depends on 15)

Device according to claim 15 wherein the temperature probe extends in the extractor tube of the tubular rod.

### Claim 17 (depends on 3)

Apparatus according to claim 3, including at least one suction means connected to the extractor tube and to an analysis system, means for injecting oxygenated gas in the furnace, and adjustable means for feeding oxygenated gas coupled to the analysis system.

### Claim 18 (depends on 3)

Apparatus according to claim 3 wherein the arc furnace includes a movable vault provided with a fumes duct section which is placed, in operating position, opposite and near a duct for the transfer of fumes, the tubular rod being disposed in the inner space between the opposite ends of the fumes duct section and of the transfer duct.

### Claim 19 (depends on 4)

The apparatus of claim 4, further comprising at least an analysis system and at least one suction means connected to the extractor tube and to the analysis system.

### Claim 20 (depends on 19)

The apparatus of claim 19, wherein the arc furnace comprises at least one gas injector and further comprising gas regulating means operatively coupled to the analysis system for selectively supplying at least one gas to the gas injector.

### Claim 21 (depends on 20)

The apparatus of claim 20, further comprising a source of oxygen-rich gas for supplying the gas injector via the gas regulating means.