# US 5,343,740 A · High sensitivity leak detection method and apparatus > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 5,343,740 A - Document ID: US5343740A - Status: Granted - Kind: A - Application number: 08/113,718 - Filed: 1993-08-27 - Granted: 1994-09-06 - Earliest claimed: 1993-08-27 - Assignees: Southeastern Universities Research Association - Inventors: Ganapatic R. Myneni - Web page: https://patentgrep.com/patent/US5343740A ## CPC - G01M 3/202: {using mass spectrometer detection systems} - F04B 37/08: by condensing or freezing, e.g. cryogenic pumps - G01M: TESTING STATIC OR DYNAMIC BALANCE OF MACHINES OR STRUCTURES; TESTING OF STRUCTURES OR APPARATUS, NOT OTHERWISE PROVIDED FOR - F04B: POSITIVE-DISPLACEMENT MACHINES FOR LIQUIDS; PUMPS (machines for liquids, or pumps, of rotary-piston or oscillating-piston type F04C; non-positive-displacement pumps F04D; pumping of fluid by direct contact of another fluid or by using inertia of fluid to be pumped F04F) ## Abstract An improved leak detection method is provided that utilizes the cyclic adsorption and desorption of accumulated helium on a non-porous metallic surface. The method provides reliable leak detection at superfluid helium temperatures. The zero drift that is associated with residual gas analyzers in common leak detectors is virtually eliminated by utilizing a time integration technique. The sensitivity of the apparatus of this disclosure is capable of detecting leaks as small as 1.times.10.sup.-18 atm cc sec.sup.-1. ## Claims ### Claim 1 An apparatus for detecting leaks from a test object comprising: a vacuum line for connecting to a test station where a test sample may be placed for determining leakage of helium by said test sample; a vacuum pump connected to said vacuum line for creating a vacuum at the test station on one side of a test sample being tested in said test station; a scavenger module connected to said test station for receiving gases leaking through a test sample in said test station and capable of removing all of said gases except helium; a helium adsorber/desorber associated with said scavenger for cyclically adsorbing said helium and desorbing said helium a multiple number of times; a non-porous thermally conducting surface in said helium adsorber/desorber on to which said helium will be cyclically adsorbed and desorbed; a source of cooling to cool said thermally conducting surface to a temperature of approximately 9 K or lower; a heater for said thermally conducting surface to heat said surface to 10 K to 20 K; and a residual gas analyzer for measuring the amount of helium present during a desorption cycle. ### Claim 2 (depends on 1) The apparatus of claim 1 wherein said scavenger module contains a cryopump with a surface held at a temperature for freezing all gases except helium and hydrogen and includes a porous adsorber for adsorbing hydrogen, ### Claim 3 (depends on 2) The apparatus of claim 2 wherein: said surface of said cryopump is held at approximately 20 K; and a second surface of said cryopump is held at a temperature of approximately 70 K for freezing gases that freeze at that temperature, ### Claim 4 (depends on 2) The apparatus of claim 2 wherein said residual gas analyzer is a mass spectrometer and said porous adsorber is carbon. ### Claim 5 (depends on 4) The apparatus of claim 4 wherein said thermally conducting surface is a copper plate. ### Claim 6 (depends on 1) The apparatus of claim 1 wherein said surface of said cryopump is held at a temperature of approximately 30 K. ### Claim 7 (depends on 1) The apparatus of claim 1 wherein: said scavenger module contains a cryopump with a cold surface for freezing all gases except helium and hydrogen; and a hydrogen molecule getter associated with said cryopump. ### Claim 8 (depends on 1) The apparatus of claim 1 wherein said thermally conducting surface is a copper plate. ### Claim 9 A method for detecting leaks from a test object comprising the following steps: providing a test station; placing a test sample on said test station; providing a vacuum pump connected to said test station; providing a scavenger module for receiving and removing all leaking gases from said test sample except helium with said scavenger module including an associated heated and cooled non-porous thermally conducting surface for adsorbing and desorbing helium; drawing a vacuum on said test sample; providing helium to leak through the said test sample; scavenging all the gases leaking through said test sample except helium; adsorbing helium on said non-porous thermally conducting surface held at approximately 9 K or lower; desorbing the helium from said non-porous thermally conducting surface by heating said non-porous thermally conducting surface to 10 K to 20 K; measuring the amount of helium desorbed from said non-porous thermally conducting surface; and repeating said cycle of adsorbing and desorbing/measuring said helium by cooling and heating said non-porous thermally conducting surface between approximately 9 K or lower and 10 K to 20 K. ### Claim 10 (depends on 9) The method of claim 9 wherein said scavenger module contains a cryopump with a surface held at a temperature for freezing all gases except helium and hydrogen and includes a porous adsorbing hydrogen. ### Claim 11 (depends on 10) The method of claim 10 wherein: said surface of said cryopump is held at approximately 20 K; and a second surface of said cryopump is held at a temperature of approximately 70 K for freezing gases that freeze at that temperature. ### Claim 12 (depends on 11) The method of claim 11 wherein said cycle of adsorbing and desorbing/measuring is repeated at least five times. ### Claim 13 (depends on 10) The method of claim 10 wherein said residual gas analyzer is a mass spectrometer and said porous adsorber is carbon. ### Claim 14 (depends on 13) The method of claim 13 wherein said thermally conducting surface is a copper plate. ### Claim 15 (depends on 14) The method of claim 14 wherein said cycle of adsorbing and desorbing/measuring is repeated at least five times. ### Claim 16 (depends on 13) The method of claim 13 wherein said cycle of adsorbing and desorbing/measuring is repeated at least five times. ### Claim 17 (depends on 9) The method of claim 9 wherein said surface of said cryopump is held at a temperature of 10 K to 20 K. ### Claim 18 (depends on 9) The method of claim 9 wherein said scavenger module contains a cryopump with a cold surface for freezing all gases except helium and hydrogen and also contains a hydrogen molecule getter for removing hydrogen. ### Claim 19 (depends on 18) The method of claim 18 wherein said cycle of adsorbing and desorbing/measuring is repeated at least five times. ### Claim 20 (depends on 9) The method of claim 9 wherein said thermally conducting surface is a copper plate.