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US 5,338,334 AGranted
Process for preparing submicron/nanosize ceramic powders from precursors incorporated within a polymeric foam
AssigneeInstitute of Gas Technology
InventorsYong S. Zhen, Kenneth Hrdina
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Abstract
A for preparing uniform, agglomerate free, submicron/nanosize ceramic powders from a polymeric foam comprising metal cations homogeneously incorporated within a foam cell structure of the polymeric foam. The polymeric foam is heated to remove any solvent, and calcined at a temperature of about 400.degree. C. to about 1400.degree. C. for about 1 minute to about 96 hours to produce the desired ceramic or metal powder.
Claims13
A process for producing at least one of ceramic powders and metal powders comprising:
- mixing an aqueous solution comprising at least one metal cation salt with an organic binder and a surfactant producing a metal salt/organic binder/surfactant mixture, said organic binder decomposing at a temperature below the melting temperature of said organic binder;
- generating gas bubbles within said metal salt/organic binder/surfactant mixture, thus forming a wet foam structure;
- drying said wet foam structure, thus forming a polymeric foam comprising homogeneously incorporated metal cations;
- calcining said polymeric foam at a calcination temperature and a time required for complete removal of all organics and formation of a crystal phase, producing at least one of an oxide powder and a metal powder;
- and
- recovering said powder.
3 more elements
Dependencies are inferred from the claim text.