Method of using an electron capture type detector
AssigneeShimadzu Corporation
InventorsToyoaki Fukushima, Shozo Tanabe
Life of this patent
Estimating the term…
Loading patent…
AssigneeShimadzu Corporation
InventorsToyoaki Fukushima, Shozo Tanabe
Estimating the term…
An electron capture type detector for gas chromatography has an ionization vessel containing therein line sources for a radioactive isotope serving as a negative electrode, a collector electrode, a purge gas route, a discharge gas route, and an end of a column disposed at its lower section. The collector electrode includes a filament made of a heat resistant material and itself connected to a heating device such that the filament can be heated to about 300.degree.-600.degree. C. so as to eliminate contaminants deposited on the collector electrode by thermal decomposition, oxidation or reduction, without the necessity of disassembling the detector itself. The contaminants are effectively removed by simultaneously causing air or hydrogen gas to pass over the collector electrode through the ionization vessel from the purge gas route to the discharge gas route.
A method of operating an electron capture type detector, said detector comprising an ionization vessel having therein line sources for a radioactive isotope serving as a negative electrode, a collector electrode, a purge gas route and a discharge gas route, and having an end of a column disposed at a lower section of said ionization vessel, said method comprising the steps of:
Dependencies are inferred from the claim text.